Enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites
In this study, magnetic polymer nanocomposite comprising of polylactide, liquified natural rubber and different loadings of NiZn ferrite nanoparticles was prepared using ultrasonication-assisted melt compounding method. The fabrication process has involved the ultrasonication treatment of the nanoco...
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oai:doaj.org-article:bb14dc6f09514765bc609b62fbb486842021-11-28T04:32:38ZEnhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites2238-785410.1016/j.jmrt.2021.11.046https://doaj.org/article/bb14dc6f09514765bc609b62fbb486842021-11-01T00:00:00Zhttp://www.sciencedirect.com/science/article/pii/S2238785421013284https://doaj.org/toc/2238-7854In this study, magnetic polymer nanocomposite comprising of polylactide, liquified natural rubber and different loadings of NiZn ferrite nanoparticles was prepared using ultrasonication-assisted melt compounding method. The fabrication process has involved the ultrasonication treatment of the nanocomposite for 1 and 2 h. The influence of ultrasonication on the dispersion degree of the nanoparticles and its reflection on the behaviour of PLA/LNR/NiZn nanocomposites was evaluated. The tensile properties showed an improvement when the nanocomposites were treated for 1 and 2 h, with optimum values obtained at 4 wt% of nanofiller loading. Similarly, the optimum values of Tg, Tc and Tm obtained from DSC analysis were found for sample ultrasonically treated for 1 h with highest crystallinity increment of 55.16% as compared to untreated sample of the same nanofiller loading. Moreover, the statistical analysis based on TGA and SEM results revealed that the nanocomposite treated ultrasonically for 1 h had better nanofiller dispersion as compared to its counterparts with 0 and 2 h treatment periods. These findings, as confirmed by magnetic testing, formed a solid evidence that the optimal behaviour of PLA/LNR/NiZn nanocomposites was attained with ultrasonication treatment of 1 h with potential applications in areas served by soft magnetic materials.Dalila ShahdanMoayad Husein FlaifelSahrim Haji AhmadRuey Shan ChenJeefferie Abd RazakElsevierarticlePolymer nanocompositesNatural rubberNanoparticlesPolylactideMechanical propertiesMagnetic propertiesMining engineering. MetallurgyTN1-997ENJournal of Materials Research and Technology, Vol 15, Iss , Pp 5988-6000 (2021) |
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Polymer nanocomposites Natural rubber Nanoparticles Polylactide Mechanical properties Magnetic properties Mining engineering. Metallurgy TN1-997 |
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Polymer nanocomposites Natural rubber Nanoparticles Polylactide Mechanical properties Magnetic properties Mining engineering. Metallurgy TN1-997 Dalila Shahdan Moayad Husein Flaifel Sahrim Haji Ahmad Ruey Shan Chen Jeefferie Abd Razak Enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites |
description |
In this study, magnetic polymer nanocomposite comprising of polylactide, liquified natural rubber and different loadings of NiZn ferrite nanoparticles was prepared using ultrasonication-assisted melt compounding method. The fabrication process has involved the ultrasonication treatment of the nanocomposite for 1 and 2 h. The influence of ultrasonication on the dispersion degree of the nanoparticles and its reflection on the behaviour of PLA/LNR/NiZn nanocomposites was evaluated. The tensile properties showed an improvement when the nanocomposites were treated for 1 and 2 h, with optimum values obtained at 4 wt% of nanofiller loading. Similarly, the optimum values of Tg, Tc and Tm obtained from DSC analysis were found for sample ultrasonically treated for 1 h with highest crystallinity increment of 55.16% as compared to untreated sample of the same nanofiller loading. Moreover, the statistical analysis based on TGA and SEM results revealed that the nanocomposite treated ultrasonically for 1 h had better nanofiller dispersion as compared to its counterparts with 0 and 2 h treatment periods. These findings, as confirmed by magnetic testing, formed a solid evidence that the optimal behaviour of PLA/LNR/NiZn nanocomposites was attained with ultrasonication treatment of 1 h with potential applications in areas served by soft magnetic materials. |
format |
article |
author |
Dalila Shahdan Moayad Husein Flaifel Sahrim Haji Ahmad Ruey Shan Chen Jeefferie Abd Razak |
author_facet |
Dalila Shahdan Moayad Husein Flaifel Sahrim Haji Ahmad Ruey Shan Chen Jeefferie Abd Razak |
author_sort |
Dalila Shahdan |
title |
Enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites |
title_short |
Enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites |
title_full |
Enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites |
title_fullStr |
Enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites |
title_full_unstemmed |
Enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of PLA/LNR/NiZn nanocomposites |
title_sort |
enhanced magnetic nanoparticles dispersion effect on the behaviour of ultrasonication-assisted compounding processing of pla/lnr/nizn nanocomposites |
publisher |
Elsevier |
publishDate |
2021 |
url |
https://doaj.org/article/bb14dc6f09514765bc609b62fbb48684 |
work_keys_str_mv |
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