Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose

This study was focused on the preparation of an environmentally friendly nanocellulose based hydrogel in the form of pads. Hydrogels are hydrophilic three dimensional network with crosslinks, swells in water but don’t dissolve. In this research nanofibrillated cellulose and Hydroxyethyl cellulose wi...

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Autores principales:	Nazanin Motie, Mehdi Jonobi, Mohammad Mehdi Faezipour, Assunta Borzacchiello
Formato:	article
Lenguaje:	FA
Publicado:	Regional Information Center for Science and Technology (RICeST) 2018
Materias:	Biohydrogel Nanocellulose swelling Thermal properties Rheology Forestry SD1-669.5
Acceso en línea:	https://doaj.org/article/c48e6f94e7224d738666ee72c9e3da14
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spelling	oai:doaj.org-article:c48e6f94e7224d738666ee72c9e3da142021-12-02T05:27:33ZInvestigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose1735-09132383-112X10.22092/ijwpr.2018.121609.1473https://doaj.org/article/c48e6f94e7224d738666ee72c9e3da142018-06-01T00:00:00Zhttp://ijwpr.areeo.ac.ir/article_116672_c43dbef50689b5716186258d111127af.pdfhttps://doaj.org/toc/1735-0913https://doaj.org/toc/2383-112XThis study was focused on the preparation of an environmentally friendly nanocellulose based hydrogel in the form of pads. Hydrogels are hydrophilic three dimensional network with crosslinks, swells in water but don’t dissolve. In this research nanofibrillated cellulose and Hydroxyethyl cellulose with different ratio (1:1, 2:1, 3:1) were used to make hydrogel. Also, citric acid which has a significant advantage over other crosslinking agents in terms of toxicity and price, has been used in different amounts of 10% and 20% by weight to crosslink. In order to find optimal hydrogel preparation conditions, FTIR analysis, FESEM, time dependent swelling measurement and evaluating the thermal and rheological properties were performed. Samples with a lower ratio of nanocellulose to hydroxyethyl cellulose were found to be inappropriate due to the loss of their apparent integrity in the swelling measurement. According to FTIR results, cross-linking were performed only in samples with the highest ratio of nanocellulose to hydroxyethyl cellulose in different amounts of citric acid. Therefore, the hydrogels' characteristics were mainly influenced by the ratio of nanocellulose to hydroxyethyl cellulose and the amount of citric acid had less effect on these properties. These two successful final samples showed acceptable properties in other evaluated properties and led to the selection of optimal reactive ratios for the preparation of hydrogels for use in various industries, including the pharmaceutical industry.Nazanin MotieMehdi JonobiMohammad Mehdi FaezipourAssunta BorzacchielloRegional Information Center for Science and Technology (RICeST)articleBiohydrogelNanocelluloseswellingThermal propertiesRheologyForestrySD1-669.5FAتحقیقات علوم چوب و کاغذ ایران, Vol 33, Iss 2, Pp 300-310 (2018)
institution	DOAJ
collection	DOAJ
language	FA
topic	Biohydrogel Nanocellulose swelling Thermal properties Rheology Forestry SD1-669.5
spellingShingle	Biohydrogel Nanocellulose swelling Thermal properties Rheology Forestry SD1-669.5 Nazanin Motie Mehdi Jonobi Mohammad Mehdi Faezipour Assunta Borzacchiello Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose
description	This study was focused on the preparation of an environmentally friendly nanocellulose based hydrogel in the form of pads. Hydrogels are hydrophilic three dimensional network with crosslinks, swells in water but don’t dissolve. In this research nanofibrillated cellulose and Hydroxyethyl cellulose with different ratio (1:1, 2:1, 3:1) were used to make hydrogel. Also, citric acid which has a significant advantage over other crosslinking agents in terms of toxicity and price, has been used in different amounts of 10% and 20% by weight to crosslink. In order to find optimal hydrogel preparation conditions, FTIR analysis, FESEM, time dependent swelling measurement and evaluating the thermal and rheological properties were performed. Samples with a lower ratio of nanocellulose to hydroxyethyl cellulose were found to be inappropriate due to the loss of their apparent integrity in the swelling measurement. According to FTIR results, cross-linking were performed only in samples with the highest ratio of nanocellulose to hydroxyethyl cellulose in different amounts of citric acid. Therefore, the hydrogels' characteristics were mainly influenced by the ratio of nanocellulose to hydroxyethyl cellulose and the amount of citric acid had less effect on these properties. These two successful final samples showed acceptable properties in other evaluated properties and led to the selection of optimal reactive ratios for the preparation of hydrogels for use in various industries, including the pharmaceutical industry.
format	article
author	Nazanin Motie Mehdi Jonobi Mohammad Mehdi Faezipour Assunta Borzacchiello
author_facet	Nazanin Motie Mehdi Jonobi Mohammad Mehdi Faezipour Assunta Borzacchiello
author_sort	Nazanin Motie
title	Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose
title_short	Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose
title_full	Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose
title_fullStr	Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose
title_full_unstemmed	Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose
title_sort	investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose
publisher	Regional Information Center for Science and Technology (RICeST)
publishDate	2018
url	https://doaj.org/article/c48e6f94e7224d738666ee72c9e3da14
work_keys_str_mv	AT nazaninmotie investigatingtheeffectofbutanedioldiglycidyletheronthecrosslinkingofnanocellulose AT mehdijonobi investigatingtheeffectofbutanedioldiglycidyletheronthecrosslinkingofnanocellulose AT mohammadmehdifaezipour investigatingtheeffectofbutanedioldiglycidyletheronthecrosslinkingofnanocellulose AT assuntaborzacchiello investigatingtheeffectofbutanedioldiglycidyletheronthecrosslinkingofnanocellulose
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Investigating the effect of butanediol diglycidyl ether on the crosslinking of nanocellulose

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