3D-structured supports create complete data sets for electron crystallography

3D electron crystallography enables structure determination of submicron-sized crystals, but obtaining complete data is difficult due to preferred orientations. Here the authors develop sample supports that allow sampling nanocrystals with full data completeness, and demonstrate this with ZSM-5 zeol...

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Autores principales: Julian T. C. Wennmacher, Christian Zaubitzer, Teng Li, Yeon Kyoung Bahk, Jing Wang, Jeroen A. van Bokhoven, Tim Gruene
Formato: article
Lenguaje:EN
Publicado: Nature Portfolio 2019
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Acceso en línea:https://doaj.org/article/c4f15532288141a5ab55872684413cf2
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Sumario:3D electron crystallography enables structure determination of submicron-sized crystals, but obtaining complete data is difficult due to preferred orientations. Here the authors develop sample supports that allow sampling nanocrystals with full data completeness, and demonstrate this with ZSM-5 zeolites.