Activated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded

The amount of loaded Co-Mo metal on the Y-Zeolite Ultra Stable (USY) was increased by the addition of activated carbon in the pre-impregnation process. USY modification was done by adding activated carbon to USY as much as 10 wt%. The process of adding activated carbon is carried out by three method...

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Autores principales: Yuniawan Hidayat, Khoirina Dwi Nugrahaningtyas, Priska Julia Hendrastuti
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Publicado: Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalas 2021
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Acceso en línea:https://doaj.org/article/c6a62ebfe566444e98b0f5fa7c5554a2
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spelling oai:doaj.org-article:c6a62ebfe566444e98b0f5fa7c5554a22021-12-02T18:47:31ZActivated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded1978-628X2476-896010.25077/jrk.v12i2.384https://doaj.org/article/c6a62ebfe566444e98b0f5fa7c5554a22021-09-01T00:00:00Zhttp://jrk.fmipa.unand.ac.id/index.php/jrk/article/view/384https://doaj.org/toc/1978-628Xhttps://doaj.org/toc/2476-8960The amount of loaded Co-Mo metal on the Y-Zeolite Ultra Stable (USY) was increased by the addition of activated carbon in the pre-impregnation process. USY modification was done by adding activated carbon to USY as much as 10 wt%. The process of adding activated carbon is carried out by three methods, i.e., grinding with sucrose binder (ACU1), without sucrose (ACU2), and conducting by ball milling (ACU3). Wet impregnation method was employed to disperse the Co and Mo, sequentially. Composites were characterized using Fourier Transform Infrared (FTIR), X-ray diffraction (XRD), and surface area analyzer (SAA). Metal dispersions were observed by X-ray fluorescence (XRF). The FTIR suggests an interaction between USY and activated car-bon, while the XRD result indicated the none structural transformation of USY zeolite. The SAA analysis showed an increased total pore radius with the activated carbon addition. The XRF confirmed the increasing of total metals dispersion of 6.25% (ACU1); 5.48%(ACU2); 5.18% (ACU3); compare to USY origin with 3.28% metals loaded.Yuniawan HidayatKhoirina Dwi NugrahaningtyasPriska Julia HendrastutiDepartment of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalasarticleactivated carbonusypre-impregnationcomoChemistryQD1-999BiochemistryQD415-436ENIDJurnal Riset Kimia, Vol 12, Iss 2 (2021)
institution DOAJ
collection DOAJ
language EN
ID
topic activated carbon
usy
pre-impregnation
co
mo
Chemistry
QD1-999
Biochemistry
QD415-436
spellingShingle activated carbon
usy
pre-impregnation
co
mo
Chemistry
QD1-999
Biochemistry
QD415-436
Yuniawan Hidayat
Khoirina Dwi Nugrahaningtyas
Priska Julia Hendrastuti
Activated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded
description The amount of loaded Co-Mo metal on the Y-Zeolite Ultra Stable (USY) was increased by the addition of activated carbon in the pre-impregnation process. USY modification was done by adding activated carbon to USY as much as 10 wt%. The process of adding activated carbon is carried out by three methods, i.e., grinding with sucrose binder (ACU1), without sucrose (ACU2), and conducting by ball milling (ACU3). Wet impregnation method was employed to disperse the Co and Mo, sequentially. Composites were characterized using Fourier Transform Infrared (FTIR), X-ray diffraction (XRD), and surface area analyzer (SAA). Metal dispersions were observed by X-ray fluorescence (XRF). The FTIR suggests an interaction between USY and activated car-bon, while the XRD result indicated the none structural transformation of USY zeolite. The SAA analysis showed an increased total pore radius with the activated carbon addition. The XRF confirmed the increasing of total metals dispersion of 6.25% (ACU1); 5.48%(ACU2); 5.18% (ACU3); compare to USY origin with 3.28% metals loaded.
format article
author Yuniawan Hidayat
Khoirina Dwi Nugrahaningtyas
Priska Julia Hendrastuti
author_facet Yuniawan Hidayat
Khoirina Dwi Nugrahaningtyas
Priska Julia Hendrastuti
author_sort Yuniawan Hidayat
title Activated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded
title_short Activated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded
title_full Activated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded
title_fullStr Activated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded
title_full_unstemmed Activated Carbon Addition Methods on the Pre-impregnation Process of Co-Mo in Y-Zeolite Ultra Stable: A Properties Exploration and Enhancement of Metals Loaded
title_sort activated carbon addition methods on the pre-impregnation process of co-mo in y-zeolite ultra stable: a properties exploration and enhancement of metals loaded
publisher Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalas
publishDate 2021
url https://doaj.org/article/c6a62ebfe566444e98b0f5fa7c5554a2
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