Analysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods

The authors of this paper have attempted to improve the quality of surface layers applied to steel elements of machine parts constituting friction couples. The main goal of the research was to investigate an electrospark alloying method process for obtaining abrasion-resistant tribological coatings...

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Autores principales: Oksana P. Gaponova, Bogdan Antoszewski, Viacheslav B. Tarelnyk, Piotr Kurp, Oleksandr M. Myslyvchenko, Nataliia V. Tarelnyk
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spelling oai:doaj.org-article:d0b11129777e41e2aac59710d7eb93b52021-11-11T17:54:11ZAnalysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods10.3390/ma142163321996-1944https://doaj.org/article/d0b11129777e41e2aac59710d7eb93b52021-10-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/21/6332https://doaj.org/toc/1996-1944The authors of this paper have attempted to improve the quality of surface layers applied to steel elements of machine parts constituting friction couples. The main goal of the research was to investigate an electrospark alloying method process for obtaining abrasion-resistant tribological coatings containing molybdenum disulfide on a steel surface. A substance in the form of sulfur ointment with a sulfur content of 33.3% was applied on the surfaces of C22 and C40 steel specimens. In order to determine the influence of the energy parameters of ESA equipment on the quality parameters of coatings, the ESA process was carried out using a molybdenum electrode with discharge energies Wp = 0.13; Wp = 0.55; Wp = 3.4 J. The following tests were carried out on specimens with such coatings: metallographic analysis, microhardness tests, surface roughness, and local X-ray diffraction microanalysis. The experiments revealed that sulfomolybdenum coatings consist of four zones with different mechanical properties. Depending on the discharge energy and the substrate material, the hardness of these zones varies from approx. 1100 to over 10,000 MPa. Differences in the distribution of, among others, sulfur and molybdenum in the obtained coatings, as well as differences in the microstructure of the observed coatings, were observed.Oksana P. GaponovaBogdan AntoszewskiViacheslav B. TarelnykPiotr KurpOleksandr M. MyslyvchenkoNataliia V. TarelnykMDPI AGarticleelectrospark alloyingsulfomolybdenum coatingstribologyTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6332, p 6332 (2021)
institution DOAJ
collection DOAJ
language EN
topic electrospark alloying
sulfomolybdenum coatings
tribology
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle electrospark alloying
sulfomolybdenum coatings
tribology
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
Oksana P. Gaponova
Bogdan Antoszewski
Viacheslav B. Tarelnyk
Piotr Kurp
Oleksandr M. Myslyvchenko
Nataliia V. Tarelnyk
Analysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods
description The authors of this paper have attempted to improve the quality of surface layers applied to steel elements of machine parts constituting friction couples. The main goal of the research was to investigate an electrospark alloying method process for obtaining abrasion-resistant tribological coatings containing molybdenum disulfide on a steel surface. A substance in the form of sulfur ointment with a sulfur content of 33.3% was applied on the surfaces of C22 and C40 steel specimens. In order to determine the influence of the energy parameters of ESA equipment on the quality parameters of coatings, the ESA process was carried out using a molybdenum electrode with discharge energies Wp = 0.13; Wp = 0.55; Wp = 3.4 J. The following tests were carried out on specimens with such coatings: metallographic analysis, microhardness tests, surface roughness, and local X-ray diffraction microanalysis. The experiments revealed that sulfomolybdenum coatings consist of four zones with different mechanical properties. Depending on the discharge energy and the substrate material, the hardness of these zones varies from approx. 1100 to over 10,000 MPa. Differences in the distribution of, among others, sulfur and molybdenum in the obtained coatings, as well as differences in the microstructure of the observed coatings, were observed.
format article
author Oksana P. Gaponova
Bogdan Antoszewski
Viacheslav B. Tarelnyk
Piotr Kurp
Oleksandr M. Myslyvchenko
Nataliia V. Tarelnyk
author_facet Oksana P. Gaponova
Bogdan Antoszewski
Viacheslav B. Tarelnyk
Piotr Kurp
Oleksandr M. Myslyvchenko
Nataliia V. Tarelnyk
author_sort Oksana P. Gaponova
title Analysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods
title_short Analysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods
title_full Analysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods
title_fullStr Analysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods
title_full_unstemmed Analysis of the Quality of Sulfomolybdenum Coatings Obtained by Electrospark Alloying Methods
title_sort analysis of the quality of sulfomolybdenum coatings obtained by electrospark alloying methods
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/d0b11129777e41e2aac59710d7eb93b5
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AT bogdanantoszewski analysisofthequalityofsulfomolybdenumcoatingsobtainedbyelectrosparkalloyingmethods
AT viacheslavbtarelnyk analysisofthequalityofsulfomolybdenumcoatingsobtainedbyelectrosparkalloyingmethods
AT piotrkurp analysisofthequalityofsulfomolybdenumcoatingsobtainedbyelectrosparkalloyingmethods
AT oleksandrmmyslyvchenko analysisofthequalityofsulfomolybdenumcoatingsobtainedbyelectrosparkalloyingmethods
AT nataliiavtarelnyk analysisofthequalityofsulfomolybdenumcoatingsobtainedbyelectrosparkalloyingmethods
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