Undulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals

The step structure on the (000<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics&g...

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Autores principales: Hiroaki Shinya, Masataka Nakano, Noboru Ohtani
Formato: article
Lenguaje:EN
Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:d235f1cc401248b1bd624ac4a956d0bb2021-11-25T18:13:51ZUndulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals10.3390/ma142268161996-1944https://doaj.org/article/d235f1cc401248b1bd624ac4a956d0bb2021-11-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/22/6816https://doaj.org/toc/1996-1944The step structure on the (000<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>)C facet of 4H-SiC boules grown by the physical vapor transport growth method with different nitrogen doping concentrations was examined in various scales, using different types of microscopy, such as differential interference contrast optical microscopy (DICM) and atomic force microscopy (AFM). DICM observations unveiled characteristic macroscopic surface features of the facet dependent on the nitrogen doping concentration. AFM observations revealed the existence of step trains of half unit-cell height (0.5 nm) on the facet and found that their separation was undulated with a characteristic wavelength dependent on the nitrogen doping concentration; the higher the nitrogen concentration, the longer was the undulation wavelength of step separation. Based on these results, we discussed the origin and formation mechanism of the separation-undulated step structure observed on the (000<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>)C facet of nitrogen-doped 4H-SiC boules.Hiroaki ShinyaMasataka NakanoNoboru OhtaniMDPI AGarticlesilicon carbidefacetstep structurenitrogen dopingstep bunchingTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6816, p 6816 (2021)
institution DOAJ
collection DOAJ
language EN
topic silicon carbide
facet
step structure
nitrogen doping
step bunching
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle silicon carbide
facet
step structure
nitrogen doping
step bunching
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
Hiroaki Shinya
Masataka Nakano
Noboru Ohtani
Undulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals
description The step structure on the (000<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>)C facet of 4H-SiC boules grown by the physical vapor transport growth method with different nitrogen doping concentrations was examined in various scales, using different types of microscopy, such as differential interference contrast optical microscopy (DICM) and atomic force microscopy (AFM). DICM observations unveiled characteristic macroscopic surface features of the facet dependent on the nitrogen doping concentration. AFM observations revealed the existence of step trains of half unit-cell height (0.5 nm) on the facet and found that their separation was undulated with a characteristic wavelength dependent on the nitrogen doping concentration; the higher the nitrogen concentration, the longer was the undulation wavelength of step separation. Based on these results, we discussed the origin and formation mechanism of the separation-undulated step structure observed on the (000<inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>)C facet of nitrogen-doped 4H-SiC boules.
format article
author Hiroaki Shinya
Masataka Nakano
Noboru Ohtani
author_facet Hiroaki Shinya
Masataka Nakano
Noboru Ohtani
author_sort Hiroaki Shinya
title Undulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals
title_short Undulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals
title_full Undulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals
title_fullStr Undulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals
title_full_unstemmed Undulated Step Structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) Facet of Physical Vapor Transport-Grown 4H-SiC Crystals
title_sort undulated step structure on the (000<inline-formula><math display="inline"><semantics><mrow><mover><mn>1</mn><mo stretchy="false">¯</mo></mover></mrow></semantics></math></inline-formula>) facet of physical vapor transport-grown 4h-sic crystals
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/d235f1cc401248b1bd624ac4a956d0bb
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AT masatakanakano undulatedstepstructureonthe000inlineformulamathdisplayinlinesemanticsmrowmovermn1mnmostretchyfalsemomovermrowsemanticsmathinlineformulafacetofphysicalvaportransportgrown4hsiccrystals
AT noboruohtani undulatedstepstructureonthe000inlineformulamathdisplayinlinesemanticsmrowmovermn1mnmostretchyfalsemomovermrowsemanticsmathinlineformulafacetofphysicalvaportransportgrown4hsiccrystals
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