Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO2 and Al2O3 Modified with APTES (3-aminopropyltriethoxysilane)

This paper describes the effect of calcination temperature on the phase composition, chemical composition, and morphology of ZrO2 and Al2O3 powders modified with 3-aminopropyltriethoxysilane (APTES). Both ceramic powders were modif...

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Autores principales:	Damian S. Nakonieczny, Frank Kern, Lukas Dufner, Agnieszka Dubiel, Magdalena Antonowicz, Krzysztof Matus
Formato:	article
Lenguaje:	EN
Publicado:	MDPI AG 2021
Materias:	zirconia alumina 3-aminopropyltriethoxysilane thermal properties surface modification Technology T Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85
Acceso en línea:	https://doaj.org/article/d27bc83067df45899d8d3fd7f7fc0efb
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spelling	oai:doaj.org-article:d27bc83067df45899d8d3fd7f7fc0efb2021-11-11T18:10:24ZEffect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)10.3390/ma142166511996-1944https://doaj.org/article/d27bc83067df45899d8d3fd7f7fc0efb2021-11-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/21/6651https://doaj.org/toc/1996-1944This paper describes the effect of calcination temperature on the phase composition, chemical composition, and morphology of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> powders modified with 3-aminopropyltriethoxysilane (APTES). Both ceramic powders were modified by etching in piranha solution, neutralization in ammonia water, reaction with APTES, ultrasonication, and finally calcination at 250, 350, or 450 °C. The obtained modified powders were characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, particle size distribution (PSD), scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM/EDS), and thermogravimetric analysis (TGA).Damian S. NakoniecznyFrank KernLukas DufnerAgnieszka DubielMagdalena AntonowiczKrzysztof MatusMDPI AGarticlezirconiaalumina3-aminopropyltriethoxysilanethermal propertiessurface modificationTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6651, p 6651 (2021)
institution	DOAJ
collection	DOAJ
language	EN
topic	zirconia alumina 3-aminopropyltriethoxysilane thermal properties surface modification Technology T Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85
spellingShingle	zirconia alumina 3-aminopropyltriethoxysilane thermal properties surface modification Technology T Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85 Damian S. Nakonieczny Frank Kern Lukas Dufner Agnieszka Dubiel Magdalena Antonowicz Krzysztof Matus Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)
description	This paper describes the effect of calcination temperature on the phase composition, chemical composition, and morphology of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> powders modified with 3-aminopropyltriethoxysilane (APTES). Both ceramic powders were modified by etching in piranha solution, neutralization in ammonia water, reaction with APTES, ultrasonication, and finally calcination at 250, 350, or 450 °C. The obtained modified powders were characterized using X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, particle size distribution (PSD), scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM/EDS), and thermogravimetric analysis (TGA).
format	article
author	Damian S. Nakonieczny Frank Kern Lukas Dufner Agnieszka Dubiel Magdalena Antonowicz Krzysztof Matus
author_facet	Damian S. Nakonieczny Frank Kern Lukas Dufner Agnieszka Dubiel Magdalena Antonowicz Krzysztof Matus
author_sort	Damian S. Nakonieczny
title	Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)
title_short	Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)
title_full	Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)
title_fullStr	Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)
title_full_unstemmed	Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)
title_sort	effect of calcination temperature on the phase composition, morphology, and thermal properties of zro<sub>2</sub> and al<sub>2</sub>o<sub>3</sub> modified with aptes (3-aminopropyltriethoxysilane)
publisher	MDPI AG
publishDate	2021
url	https://doaj.org/article/d27bc83067df45899d8d3fd7f7fc0efb
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_version_	1718431912434860032

Effect of Calcination Temperature on the Phase Composition, Morphology, and Thermal Properties of ZrO<sub>2</sub> and Al<sub>2</sub>O<sub>3</sub> Modified with APTES (3-aminopropyltriethoxysilane)

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