High-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite
The applicability of nano-crystalline W/Cu composites is governed by their mechanical properties and microstructural stability at high temperatures. Therefore, mechanical and structural investigations of a high-pressure torsion deformed W/Cu nanocomposite were performed up to a temperature of 600 °C...
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MDPI AG
2021
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oai:doaj.org-article:d421a500befa426b8edb8243d9ff6f1a2021-11-25T18:31:06ZHigh-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite10.3390/nano111129512079-4991https://doaj.org/article/d421a500befa426b8edb8243d9ff6f1a2021-11-01T00:00:00Zhttps://www.mdpi.com/2079-4991/11/11/2951https://doaj.org/toc/2079-4991The applicability of nano-crystalline W/Cu composites is governed by their mechanical properties and microstructural stability at high temperatures. Therefore, mechanical and structural investigations of a high-pressure torsion deformed W/Cu nanocomposite were performed up to a temperature of 600 °C. Furthermore, the material was annealed at several temperatures for 1 h within a high-vacuum furnace to determine microstructural changes and surface effects. No significant increase of grain size, but distinct evaporation of the Cu phase accompanied by Cu pool and faceted Cu particle formation could be identified on the specimen′s surface. Additionally, high-temperature nanoindentation and strain rate jump tests were performed to investigate the materials mechanical response at elevated temperatures. Hardness and Young′s modulus decrease were noteworthy due to temperature-induced effects and slight grain growth. The strain rate sensitivity in dependent of the temperature remained constant for the investigated W/Cu composite material. Also, the activation volume of the nano-crystalline composite increased with temperature and behaved similar to coarse-grained W. The current study extends the understanding of the high-temperature behavior of nano-crystalline W/Cu composites within vacuum environments such as future fusion reactors.Michael BurtscherMingyue ZhaoJohann KappacherAlexander LeitnerMichael WurmshuberManuel PfeifenbergerVerena Maier-KienerDaniel KienerMDPI AGarticleW/Cu compositenanocrystallinehigh-pressure torsionmicrostructurenanoindentationChemistryQD1-999ENNanomaterials, Vol 11, Iss 2951, p 2951 (2021) |
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W/Cu composite nanocrystalline high-pressure torsion microstructure nanoindentation Chemistry QD1-999 |
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W/Cu composite nanocrystalline high-pressure torsion microstructure nanoindentation Chemistry QD1-999 Michael Burtscher Mingyue Zhao Johann Kappacher Alexander Leitner Michael Wurmshuber Manuel Pfeifenberger Verena Maier-Kiener Daniel Kiener High-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite |
description |
The applicability of nano-crystalline W/Cu composites is governed by their mechanical properties and microstructural stability at high temperatures. Therefore, mechanical and structural investigations of a high-pressure torsion deformed W/Cu nanocomposite were performed up to a temperature of 600 °C. Furthermore, the material was annealed at several temperatures for 1 h within a high-vacuum furnace to determine microstructural changes and surface effects. No significant increase of grain size, but distinct evaporation of the Cu phase accompanied by Cu pool and faceted Cu particle formation could be identified on the specimen′s surface. Additionally, high-temperature nanoindentation and strain rate jump tests were performed to investigate the materials mechanical response at elevated temperatures. Hardness and Young′s modulus decrease were noteworthy due to temperature-induced effects and slight grain growth. The strain rate sensitivity in dependent of the temperature remained constant for the investigated W/Cu composite material. Also, the activation volume of the nano-crystalline composite increased with temperature and behaved similar to coarse-grained W. The current study extends the understanding of the high-temperature behavior of nano-crystalline W/Cu composites within vacuum environments such as future fusion reactors. |
format |
article |
author |
Michael Burtscher Mingyue Zhao Johann Kappacher Alexander Leitner Michael Wurmshuber Manuel Pfeifenberger Verena Maier-Kiener Daniel Kiener |
author_facet |
Michael Burtscher Mingyue Zhao Johann Kappacher Alexander Leitner Michael Wurmshuber Manuel Pfeifenberger Verena Maier-Kiener Daniel Kiener |
author_sort |
Michael Burtscher |
title |
High-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite |
title_short |
High-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite |
title_full |
High-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite |
title_fullStr |
High-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite |
title_full_unstemmed |
High-Temperature Nanoindentation of an Advanced Nano-Crystalline W/Cu Composite |
title_sort |
high-temperature nanoindentation of an advanced nano-crystalline w/cu composite |
publisher |
MDPI AG |
publishDate |
2021 |
url |
https://doaj.org/article/d421a500befa426b8edb8243d9ff6f1a |
work_keys_str_mv |
AT michaelburtscher hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite AT mingyuezhao hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite AT johannkappacher hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite AT alexanderleitner hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite AT michaelwurmshuber hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite AT manuelpfeifenberger hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite AT verenamaierkiener hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite AT danielkiener hightemperaturenanoindentationofanadvancednanocrystallinewcucomposite |
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