Microstructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing

A TNM alloy ingot was fabricated with powder hot isostatic pressing (P-HIP) and short-time exposure treatment conducted at 750–1050 °C for 2–5 h. The tensile mechanical properties were investigated at room temperature and 800 °C. The results revealed that a fully lamellar microstructure of P-HIPed T...

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Autores principales: Yichao Wang, Xiangyi Xue, Hongchao Kou, Fengming Qiang, Yonghao Yu, Zhongwei Yin, Jinshan Li
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Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:da8cfa3dc04c4b6497705ef2611192282021-11-25T18:21:28ZMicrostructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing10.3390/met111117202075-4701https://doaj.org/article/da8cfa3dc04c4b6497705ef2611192282021-10-01T00:00:00Zhttps://www.mdpi.com/2075-4701/11/11/1720https://doaj.org/toc/2075-4701A TNM alloy ingot was fabricated with powder hot isostatic pressing (P-HIP) and short-time exposure treatment conducted at 750–1050 °C for 2–5 h. The tensile mechanical properties were investigated at room temperature and 800 °C. The results revealed that a fully lamellar microstructure of P-HIPed TNM alloy with only 0.3 vol.% β<sub>0</sub> phase could be obtained by hot isostatic pressing at 1260 °C, under the pressure of 170 MPa, held for 4 h. When the exposure temperature was below 850 °C, the α<sub>2</sub> lamellae were transformed into nano-scaled (α<sub>2</sub> + γ) lamellae (i.e., the α<sub>2</sub>→α<sub>2</sub> + γ transformation). With increases in the exposure temperature, the β<sub>0</sub> phase began to precipitate within the α<sub>2</sub> lamellae (α<sub>2</sub>→β<sub>0</sub> transformation) at 950 °C. The α<sub>2</sub>→γ and the α<sub>2</sub>→β<sub>0</sub> transformation both happened at 950–1050 °C, and the higher exposure temperature accelerated the diffusion of Mo and facilitated the α<sub>2</sub>→β<sub>0</sub> transformation. The yield strength and elongation at RT and 800 °C were both improved after short-time high-temperature exposure treatment. The uniform distribution and nano-scaled interfacial β<sub>0</sub> phase provided precipitation strengthening and were not harmful to the elongation.Yichao WangXiangyi XueHongchao KouFengming QiangYonghao YuZhongwei YinJinshan LiMDPI AGarticleTiAl-based alloyshot isostatic pressingmicrostructurethermal stabilitytensile propertiesMining engineering. MetallurgyTN1-997ENMetals, Vol 11, Iss 1720, p 1720 (2021)
institution DOAJ
collection DOAJ
language EN
topic TiAl-based alloys
hot isostatic pressing
microstructure
thermal stability
tensile properties
Mining engineering. Metallurgy
TN1-997
spellingShingle TiAl-based alloys
hot isostatic pressing
microstructure
thermal stability
tensile properties
Mining engineering. Metallurgy
TN1-997
Yichao Wang
Xiangyi Xue
Hongchao Kou
Fengming Qiang
Yonghao Yu
Zhongwei Yin
Jinshan Li
Microstructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing
description A TNM alloy ingot was fabricated with powder hot isostatic pressing (P-HIP) and short-time exposure treatment conducted at 750–1050 °C for 2–5 h. The tensile mechanical properties were investigated at room temperature and 800 °C. The results revealed that a fully lamellar microstructure of P-HIPed TNM alloy with only 0.3 vol.% β<sub>0</sub> phase could be obtained by hot isostatic pressing at 1260 °C, under the pressure of 170 MPa, held for 4 h. When the exposure temperature was below 850 °C, the α<sub>2</sub> lamellae were transformed into nano-scaled (α<sub>2</sub> + γ) lamellae (i.e., the α<sub>2</sub>→α<sub>2</sub> + γ transformation). With increases in the exposure temperature, the β<sub>0</sub> phase began to precipitate within the α<sub>2</sub> lamellae (α<sub>2</sub>→β<sub>0</sub> transformation) at 950 °C. The α<sub>2</sub>→γ and the α<sub>2</sub>→β<sub>0</sub> transformation both happened at 950–1050 °C, and the higher exposure temperature accelerated the diffusion of Mo and facilitated the α<sub>2</sub>→β<sub>0</sub> transformation. The yield strength and elongation at RT and 800 °C were both improved after short-time high-temperature exposure treatment. The uniform distribution and nano-scaled interfacial β<sub>0</sub> phase provided precipitation strengthening and were not harmful to the elongation.
format article
author Yichao Wang
Xiangyi Xue
Hongchao Kou
Fengming Qiang
Yonghao Yu
Zhongwei Yin
Jinshan Li
author_facet Yichao Wang
Xiangyi Xue
Hongchao Kou
Fengming Qiang
Yonghao Yu
Zhongwei Yin
Jinshan Li
author_sort Yichao Wang
title Microstructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing
title_short Microstructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing
title_full Microstructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing
title_fullStr Microstructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing
title_full_unstemmed Microstructure Characterization and Thermal Stability of TNM Alloy Fabricated by Powder Hot Isostatic Pressing
title_sort microstructure characterization and thermal stability of tnm alloy fabricated by powder hot isostatic pressing
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/da8cfa3dc04c4b6497705ef261119228
work_keys_str_mv AT yichaowang microstructurecharacterizationandthermalstabilityoftnmalloyfabricatedbypowderhotisostaticpressing
AT xiangyixue microstructurecharacterizationandthermalstabilityoftnmalloyfabricatedbypowderhotisostaticpressing
AT hongchaokou microstructurecharacterizationandthermalstabilityoftnmalloyfabricatedbypowderhotisostaticpressing
AT fengmingqiang microstructurecharacterizationandthermalstabilityoftnmalloyfabricatedbypowderhotisostaticpressing
AT yonghaoyu microstructurecharacterizationandthermalstabilityoftnmalloyfabricatedbypowderhotisostaticpressing
AT zhongweiyin microstructurecharacterizationandthermalstabilityoftnmalloyfabricatedbypowderhotisostaticpressing
AT jinshanli microstructurecharacterizationandthermalstabilityoftnmalloyfabricatedbypowderhotisostaticpressing
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