A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding

Abstract The ternary compound boron carbonitride (BCN) was synthesized in the form of few-layer nanosheets through a mechanically induced self-sustaining reaction (MSR). Magnesium was used to reduce boron trioxide in the presence of melamine in a combustive manner. The process to form the nanostruct...

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Autores principales:	Maisam Jalaly, Francisco José Gotor, Masih Semnan, María Jesús Sayagués
Formato:	article
Lenguaje:	EN
Publicado:	Nature Portfolio 2017
Materias:	Medicine R Science Q
Acceso en línea:	https://doaj.org/article/dd69be6f23d9487c86c45db9f3431a7d
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spelling	oai:doaj.org-article:dd69be6f23d9487c86c45db9f3431a7d2021-12-02T16:06:15ZA novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding10.1038/s41598-017-03794-72045-2322https://doaj.org/article/dd69be6f23d9487c86c45db9f3431a7d2017-06-01T00:00:00Zhttps://doi.org/10.1038/s41598-017-03794-7https://doaj.org/toc/2045-2322Abstract The ternary compound boron carbonitride (BCN) was synthesized in the form of few-layer nanosheets through a mechanically induced self-sustaining reaction (MSR). Magnesium was used to reduce boron trioxide in the presence of melamine in a combustive manner. The process to form the nanostructured material was very rapid (less than 40 min). The prepared powder was investigated by various techniques such as X-ray diffraction (XRD), Fourier Transform infrared (FTIR), Micro-Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), high-resolution transmission electron microscopy (HRTEM), and electron energy loss spectroscopy (EELS). The thermal stability and the optical behavior of the BCN nanosheets were also studied by thermal analysis and UV-vis spectroscopy, respectively. The formation mechanism of the nanosheet morphology was described in detail.Maisam JalalyFrancisco José GotorMasih SemnanMaría Jesús SayaguésNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 7, Iss 1, Pp 1-13 (2017)
institution	DOAJ
collection	DOAJ
language	EN
topic	Medicine R Science Q
spellingShingle	Medicine R Science Q Maisam Jalaly Francisco José Gotor Masih Semnan María Jesús Sayagués A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding
description	Abstract The ternary compound boron carbonitride (BCN) was synthesized in the form of few-layer nanosheets through a mechanically induced self-sustaining reaction (MSR). Magnesium was used to reduce boron trioxide in the presence of melamine in a combustive manner. The process to form the nanostructured material was very rapid (less than 40 min). The prepared powder was investigated by various techniques such as X-ray diffraction (XRD), Fourier Transform infrared (FTIR), Micro-Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), high-resolution transmission electron microscopy (HRTEM), and electron energy loss spectroscopy (EELS). The thermal stability and the optical behavior of the BCN nanosheets were also studied by thermal analysis and UV-vis spectroscopy, respectively. The formation mechanism of the nanosheet morphology was described in detail.
format	article
author	Maisam Jalaly Francisco José Gotor Masih Semnan María Jesús Sayagués
author_facet	Maisam Jalaly Francisco José Gotor Masih Semnan María Jesús Sayagués
author_sort	Maisam Jalaly
title	A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding
title_short	A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding
title_full	A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding
title_fullStr	A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding
title_full_unstemmed	A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding
title_sort	novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding
publisher	Nature Portfolio
publishDate	2017
url	https://doaj.org/article/dd69be6f23d9487c86c45db9f3431a7d
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A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: combustive gaseous unfolding

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