Experimental methodology for bubble content measurement of thin films

The inclusion of micro bubbles often exists in polyimide films (PI) during the liquid molding process, which can largely affect the mechanical performance. However, there lacks an effective method to quantify the bubble content. Herein, an obvious tension variation of a pre-stressed polyimide film i...

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Autores principales: Yibei Zhang, Bing Zhao, Jianhui Hu, Wujun Chen, Xiaowei Deng, Zhengyue Yu, Chao Xie, Fujun Peng, Xiaofei Huang
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Lenguaje:EN
Publicado: Elsevier 2021
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Acceso en línea:https://doaj.org/article/e304a858735042428f01a6b3e9c3237b
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spelling oai:doaj.org-article:e304a858735042428f01a6b3e9c3237b2021-11-24T04:23:38ZExperimental methodology for bubble content measurement of thin films0142-941810.1016/j.polymertesting.2020.106876https://doaj.org/article/e304a858735042428f01a6b3e9c3237b2021-01-01T00:00:00Zhttp://www.sciencedirect.com/science/article/pii/S014294182032105Xhttps://doaj.org/toc/0142-9418The inclusion of micro bubbles often exists in polyimide films (PI) during the liquid molding process, which can largely affect the mechanical performance. However, there lacks an effective method to quantify the bubble content. Herein, an obvious tension variation of a pre-stressed polyimide film is observed firstly in a vacuum test. This phenomenon is assumed that, when the vacuum level of the testing environment increases, the inner bubbles would expand mainly out of plane, resulting in an in-plane contraction, and the tension varies accordingly. This tension variation ability is found quite stable despite of the stochastic micro-bubble distribution, which could be utilized to quantify the bubble content. Moreover, a film with meso-size bubbles is tested to have the similar tension variation ability. According to the experimental results, the tension variation ability can be basically stable when the bubbles in the length and width directions reach a certain number (e.g. 10).Yibei ZhangBing ZhaoJianhui HuWujun ChenXiaowei DengZhengyue YuChao XieFujun PengXiaofei HuangElsevierarticleBubble contentThin filmsTension variation testsVacuum testsMeso-size bubblesPolymers and polymer manufactureTP1080-1185ENPolymer Testing, Vol 93, Iss , Pp 106876- (2021)
institution DOAJ
collection DOAJ
language EN
topic Bubble content
Thin films
Tension variation tests
Vacuum tests
Meso-size bubbles
Polymers and polymer manufacture
TP1080-1185
spellingShingle Bubble content
Thin films
Tension variation tests
Vacuum tests
Meso-size bubbles
Polymers and polymer manufacture
TP1080-1185
Yibei Zhang
Bing Zhao
Jianhui Hu
Wujun Chen
Xiaowei Deng
Zhengyue Yu
Chao Xie
Fujun Peng
Xiaofei Huang
Experimental methodology for bubble content measurement of thin films
description The inclusion of micro bubbles often exists in polyimide films (PI) during the liquid molding process, which can largely affect the mechanical performance. However, there lacks an effective method to quantify the bubble content. Herein, an obvious tension variation of a pre-stressed polyimide film is observed firstly in a vacuum test. This phenomenon is assumed that, when the vacuum level of the testing environment increases, the inner bubbles would expand mainly out of plane, resulting in an in-plane contraction, and the tension varies accordingly. This tension variation ability is found quite stable despite of the stochastic micro-bubble distribution, which could be utilized to quantify the bubble content. Moreover, a film with meso-size bubbles is tested to have the similar tension variation ability. According to the experimental results, the tension variation ability can be basically stable when the bubbles in the length and width directions reach a certain number (e.g. 10).
format article
author Yibei Zhang
Bing Zhao
Jianhui Hu
Wujun Chen
Xiaowei Deng
Zhengyue Yu
Chao Xie
Fujun Peng
Xiaofei Huang
author_facet Yibei Zhang
Bing Zhao
Jianhui Hu
Wujun Chen
Xiaowei Deng
Zhengyue Yu
Chao Xie
Fujun Peng
Xiaofei Huang
author_sort Yibei Zhang
title Experimental methodology for bubble content measurement of thin films
title_short Experimental methodology for bubble content measurement of thin films
title_full Experimental methodology for bubble content measurement of thin films
title_fullStr Experimental methodology for bubble content measurement of thin films
title_full_unstemmed Experimental methodology for bubble content measurement of thin films
title_sort experimental methodology for bubble content measurement of thin films
publisher Elsevier
publishDate 2021
url https://doaj.org/article/e304a858735042428f01a6b3e9c3237b
work_keys_str_mv AT yibeizhang experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT bingzhao experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT jianhuihu experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT wujunchen experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT xiaoweideng experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT zhengyueyu experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT chaoxie experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT fujunpeng experimentalmethodologyforbubblecontentmeasurementofthinfilms
AT xiaofeihuang experimentalmethodologyforbubblecontentmeasurementofthinfilms
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