Heating rate effects on thermal analysis measurement of Tg in composite materials

Three measurement techniques used to measure the glass transition temperature (Tg) have been subjected to a critical comparison; dynamic mechanical analysis (DMA), thermomechanical analysis, and differential scanning calorimetry. A new procedure, whereby different specimens are tested over a range o...

Descripción completa

Guardado en:

Detalles Bibliográficos
Autores principales:	Ana X. H. Yong, Graham D. Sims, Samuel J. P. Gnaniah, Stephen L. Ogin, Paul A. Smith
Formato:	article
Lenguaje:	EN
Publicado:	Taylor & Francis Group 2017
Materias:	Thermal analysis Cure monitoring Glass transition temperature Polymer composites Polymers and polymer manufacture TP1080-1185 Automation T59.5
Acceso en línea:	https://doaj.org/article/ea36d0993da14f0d871aeff40b5b215f
Etiquetas:	Agregar Etiqueta Sin Etiquetas, Sea el primero en etiquetar este registro!

id	oai:doaj.org-article:ea36d0993da14f0d871aeff40b5b215f
record_format	dspace
spelling	oai:doaj.org-article:ea36d0993da14f0d871aeff40b5b215f2021-12-02T03:25:24ZHeating rate effects on thermal analysis measurement of Tg in composite materials2055-03402055-035910.1080/20550340.2017.1315908https://doaj.org/article/ea36d0993da14f0d871aeff40b5b215f2017-04-01T00:00:00Zhttp://dx.doi.org/10.1080/20550340.2017.1315908https://doaj.org/toc/2055-0340https://doaj.org/toc/2055-0359Three measurement techniques used to measure the glass transition temperature (Tg) have been subjected to a critical comparison; dynamic mechanical analysis (DMA), thermomechanical analysis, and differential scanning calorimetry. A new procedure, whereby different specimens are tested over a range of heating rates, has been used in order to eliminate the effects of thermal lag and determine a Tg independent of heating rate (Tg(0)). It has been shown that for measurements of Tg(0) for composites, the DMA thermal lag “corrected” method gave the most reliable data. The work has provided additional guidance on these techniques that could usefully be incorporated in future standards, to improve precision, comparisons, and consistency of Tg measurement.Ana X. H. YongGraham D. SimsSamuel J. P. GnaniahStephen L. OginPaul A. SmithTaylor & Francis GrouparticleThermal analysisCure monitoringGlass transition temperaturePolymer compositesPolymers and polymer manufactureTP1080-1185AutomationT59.5ENAdvanced Manufacturing: Polymer & Composites Science, Vol 3, Iss 2, Pp 43-51 (2017)
institution	DOAJ
collection	DOAJ
language	EN
topic	Thermal analysis Cure monitoring Glass transition temperature Polymer composites Polymers and polymer manufacture TP1080-1185 Automation T59.5
spellingShingle	Thermal analysis Cure monitoring Glass transition temperature Polymer composites Polymers and polymer manufacture TP1080-1185 Automation T59.5 Ana X. H. Yong Graham D. Sims Samuel J. P. Gnaniah Stephen L. Ogin Paul A. Smith Heating rate effects on thermal analysis measurement of Tg in composite materials
description	Three measurement techniques used to measure the glass transition temperature (Tg) have been subjected to a critical comparison; dynamic mechanical analysis (DMA), thermomechanical analysis, and differential scanning calorimetry. A new procedure, whereby different specimens are tested over a range of heating rates, has been used in order to eliminate the effects of thermal lag and determine a Tg independent of heating rate (Tg(0)). It has been shown that for measurements of Tg(0) for composites, the DMA thermal lag “corrected” method gave the most reliable data. The work has provided additional guidance on these techniques that could usefully be incorporated in future standards, to improve precision, comparisons, and consistency of Tg measurement.
format	article
author	Ana X. H. Yong Graham D. Sims Samuel J. P. Gnaniah Stephen L. Ogin Paul A. Smith
author_facet	Ana X. H. Yong Graham D. Sims Samuel J. P. Gnaniah Stephen L. Ogin Paul A. Smith
author_sort	Ana X. H. Yong
title	Heating rate effects on thermal analysis measurement of Tg in composite materials
title_short	Heating rate effects on thermal analysis measurement of Tg in composite materials
title_full	Heating rate effects on thermal analysis measurement of Tg in composite materials
title_fullStr	Heating rate effects on thermal analysis measurement of Tg in composite materials
title_full_unstemmed	Heating rate effects on thermal analysis measurement of Tg in composite materials
title_sort	heating rate effects on thermal analysis measurement of tg in composite materials
publisher	Taylor & Francis Group
publishDate	2017
url	https://doaj.org/article/ea36d0993da14f0d871aeff40b5b215f
work_keys_str_mv	AT anaxhyong heatingrateeffectsonthermalanalysismeasurementoftgincompositematerials AT grahamdsims heatingrateeffectsonthermalanalysismeasurementoftgincompositematerials AT samueljpgnaniah heatingrateeffectsonthermalanalysismeasurementoftgincompositematerials AT stephenlogin heatingrateeffectsonthermalanalysismeasurementoftgincompositematerials AT paulasmith heatingrateeffectsonthermalanalysismeasurementoftgincompositematerials
_version_	1718401829434294272

Heating rate effects on thermal analysis measurement of Tg in composite materials

Ejemplares similares