Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods

CuO nanoparticles were synthesized in two different ways, firstly by precipitation method using copper acetate monohydrate Cu(CO2CH13)2·H2O, glacial acetic acid (CH3COOH) and sodium hydroxide(NaOH), and secondly by sol-gel method using copper chloride(CuCl2), sodium hydroxide (NaOH) and ethanol (C...

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Autor principal:	Saja Mohsen Jabbar
Formato:	article
Lenguaje:	EN
Publicado:	Al-Khwarizmi College of Engineering – University of Baghdad 2017
Materias:	CuO nanostructure precipitation method sol- gel method Chemical engineering TP155-156 Engineering (General). Civil engineering (General) TA1-2040
Acceso en línea:	https://doaj.org/article/ea45be819fb949298f1081d97659c889
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spelling	oai:doaj.org-article:ea45be819fb949298f1081d97659c8892021-12-02T07:32:13ZSynthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods10.22153/kej.2016.07.0011818-11712312-0789https://doaj.org/article/ea45be819fb949298f1081d97659c8892017-12-01T00:00:00Zhttp://alkej.uobaghdad.edu.iq/index.php/alkej/article/view/327https://doaj.org/toc/1818-1171https://doaj.org/toc/2312-0789 CuO nanoparticles were synthesized in two different ways, firstly by precipitation method using copper acetate monohydrate Cu(CO2CH13)2·H2O, glacial acetic acid (CH3COOH) and sodium hydroxide(NaOH), and secondly by sol-gel method using copper chloride(CuCl2), sodium hydroxide (NaOH) and ethanol (C2H6O). Results of scanning electron microscopy (SEM) showed that different CuO nanostructures (spherical and Reef) can be formed using precipitation and sol- gel process, respectively, at which the particle size was found to be less than 2 µm. X-ray diffraction (XRD)manifested that the pure synthesized powder has no inclusions that may exist during preparations. XRD results showed the particles size of highest peak at 38.9°, was equal to (15.93nm). In addition, Fourier transform infrared spectroscopy (FT-IR) were used to describe the prepared CuO nanostructures absorption peak at 610 cm-1 which conﬁrms that the synthesized product is a pure CuO and may be attributed to Cu2O infrared active mode. Saja Mohsen JabbarAl-Khwarizmi College of Engineering – University of BaghdadarticleCuO nanostructureprecipitation methodsol- gel methodChemical engineeringTP155-156Engineering (General). Civil engineering (General)TA1-2040ENAl-Khawarizmi Engineering Journal, Vol 12, Iss 4 (2017)
institution	DOAJ
collection	DOAJ
language	EN
topic	CuO nanostructure precipitation method sol- gel method Chemical engineering TP155-156 Engineering (General). Civil engineering (General) TA1-2040
spellingShingle	CuO nanostructure precipitation method sol- gel method Chemical engineering TP155-156 Engineering (General). Civil engineering (General) TA1-2040 Saja Mohsen Jabbar Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods
description	CuO nanoparticles were synthesized in two different ways, firstly by precipitation method using copper acetate monohydrate Cu(CO2CH13)2·H2O, glacial acetic acid (CH3COOH) and sodium hydroxide(NaOH), and secondly by sol-gel method using copper chloride(CuCl2), sodium hydroxide (NaOH) and ethanol (C2H6O). Results of scanning electron microscopy (SEM) showed that different CuO nanostructures (spherical and Reef) can be formed using precipitation and sol- gel process, respectively, at which the particle size was found to be less than 2 µm. X-ray diffraction (XRD)manifested that the pure synthesized powder has no inclusions that may exist during preparations. XRD results showed the particles size of highest peak at 38.9°, was equal to (15.93nm). In addition, Fourier transform infrared spectroscopy (FT-IR) were used to describe the prepared CuO nanostructures absorption peak at 610 cm-1 which conﬁrms that the synthesized product is a pure CuO and may be attributed to Cu2O infrared active mode.
format	article
author	Saja Mohsen Jabbar
author_facet	Saja Mohsen Jabbar
author_sort	Saja Mohsen Jabbar
title	Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods
title_short	Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods
title_full	Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods
title_fullStr	Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods
title_full_unstemmed	Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods
title_sort	synthesis of cuo nano structure via sol-gel and precipitation chemical methods
publisher	Al-Khwarizmi College of Engineering – University of Baghdad
publishDate	2017
url	https://doaj.org/article/ea45be819fb949298f1081d97659c889
work_keys_str_mv	AT sajamohsenjabbar synthesisofcuonanostructureviasolgelandprecipitationchemicalmethods
_version_	1718399373917814784

Synthesis of CuO Nano structure via Sol-Gel and Precipitation Chemical Methods

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