The analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb

Abstract Recently, a bowl containing charred suspected tea remains unearthed from the early stage of Warring States period tomb in Zoucheng City, Shandong Province, China. To identify the remains is significant for understanding the origin of tea and tea drinking culture. Scientific investigations o...

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Autores principales: Jianrong Jiang, Guoquan Lu, Qing Wang, Shuya Wei
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Publicado: Nature Portfolio 2021
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Acceso en línea:https://doaj.org/article/edc0b49bf29d433fafbf4fca198436bb
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spelling oai:doaj.org-article:edc0b49bf29d433fafbf4fca198436bb2021-12-02T17:08:43ZThe analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb10.1038/s41598-021-95393-w2045-2322https://doaj.org/article/edc0b49bf29d433fafbf4fca198436bb2021-08-01T00:00:00Zhttps://doi.org/10.1038/s41598-021-95393-whttps://doaj.org/toc/2045-2322Abstract Recently, a bowl containing charred suspected tea remains unearthed from the early stage of Warring States period tomb in Zoucheng City, Shandong Province, China. To identify the remains is significant for understanding the origin of tea and tea drinking culture. Scientific investigations of the remains were carried out by using calcium phytoliths analysis, Fourier transform infrared spectroscopy (FTIR), Gas Chromatograph Mass Spectrometer (GC/MS) and Thermally assisted hydrolysis—methylation Pyrolysis Gas Chromatography Mass Spectrometry (THM-Py-GC/MS) techniques. Modern tea and modern tea residue were used as reference samples. Through phytoliths analyses, calcium phytoliths identifiable from tea were determined in the archeological remains. The infrared spectra of the archaeological remains was found similar as modern tea residue reference sample. In addition, the biomarker compound of tea—caffeine was determined in the archaeological remains by THM-Py-GC/MS analysis. Furthermore, through GC/MS analysis, some compounds were found both in the archeological remains and the modern tea residue reference samples. Putting the information together, it can be concluded that the archaeological remains in the bowl are tea residue after boiling or brewing by the ancient.Jianrong JiangGuoquan LuQing WangShuya WeiNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 11, Iss 1, Pp 1-8 (2021)
institution DOAJ
collection DOAJ
language EN
topic Medicine
R
Science
Q
spellingShingle Medicine
R
Science
Q
Jianrong Jiang
Guoquan Lu
Qing Wang
Shuya Wei
The analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb
description Abstract Recently, a bowl containing charred suspected tea remains unearthed from the early stage of Warring States period tomb in Zoucheng City, Shandong Province, China. To identify the remains is significant for understanding the origin of tea and tea drinking culture. Scientific investigations of the remains were carried out by using calcium phytoliths analysis, Fourier transform infrared spectroscopy (FTIR), Gas Chromatograph Mass Spectrometer (GC/MS) and Thermally assisted hydrolysis—methylation Pyrolysis Gas Chromatography Mass Spectrometry (THM-Py-GC/MS) techniques. Modern tea and modern tea residue were used as reference samples. Through phytoliths analyses, calcium phytoliths identifiable from tea were determined in the archeological remains. The infrared spectra of the archaeological remains was found similar as modern tea residue reference sample. In addition, the biomarker compound of tea—caffeine was determined in the archaeological remains by THM-Py-GC/MS analysis. Furthermore, through GC/MS analysis, some compounds were found both in the archeological remains and the modern tea residue reference samples. Putting the information together, it can be concluded that the archaeological remains in the bowl are tea residue after boiling or brewing by the ancient.
format article
author Jianrong Jiang
Guoquan Lu
Qing Wang
Shuya Wei
author_facet Jianrong Jiang
Guoquan Lu
Qing Wang
Shuya Wei
author_sort Jianrong Jiang
title The analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb
title_short The analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb
title_full The analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb
title_fullStr The analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb
title_full_unstemmed The analysis and identification of charred suspected tea remains unearthed from Warring State Period Tomb
title_sort analysis and identification of charred suspected tea remains unearthed from warring state period tomb
publisher Nature Portfolio
publishDate 2021
url https://doaj.org/article/edc0b49bf29d433fafbf4fca198436bb
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