Monitoring the Capillary Jet Breakage by Vibration Using a Fast-Video Camera

The production of beads by simple extrusion dropwise of an alginate solution in a calcium bath is a simple method. It may be done at room temperature without any toxic compound. However, simple extrusion drop by drop from a needle may result in large capsules and a low flow rate. The solution must b...

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Autores principales: Marcella Chalella Mazzocato, Sylvie Chevallier, Carmen S. Fávaro-Trindade, Denis Poncelet
Formato: article
Lenguaje:EN
Publicado: MDPI AG 2021
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Acceso en línea:https://doaj.org/article/f1f22d6f55db4efda19379a9876981cc
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Sumario:The production of beads by simple extrusion dropwise of an alginate solution in a calcium bath is a simple method. It may be done at room temperature without any toxic compound. However, simple extrusion drop by drop from a needle may result in large capsules and a low flow rate. The solution must be extruded as a jet to get a smaller size and higher flow rate, which breaks into droplets either by vibration or a cutting tool. The present contribution reports jet breakage observations into droplets under vibration by extruding an alginate solution varying some parameters during the study. The droplet formation was observed using a high-speed camera, and images were analyzed. The size, length before breakage, and droplet velocity were obtained by examining 50 droplets, and experiments were repeated three times. The high-speed camera allowed us to observe more precisely the capillary jet breakage. The study showed the importance of selecting a well-designed vibrating system, presented data while varying nozzle size, frequency, and flow rate to get optimum breakage keeping across all the same alginate solution. Further experiments would be interesting, modify the extruded solution concentration and composition, and find a precise criterion to identify optimum conditions.