Effect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry

The objective of this research was to evaluate the polyphenolic compounds, the antioxidant activity, and the individual identification of the different types of phenolic compounds in dried extracts of Opuntia atropes. O. atropes extract was dehydrated in a drying oven at 50°C/24 h and by nano-spray...

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Autores principales: Eunice Tranquilino-Rodríguez, Héctor E. Martínez-Flores, José O. Rodiles-López, Guillermo C.G. Martínez-Avila
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Publicado: Taylor & Francis Group 2021
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Acceso en línea:https://doaj.org/article/f70b1837e60148e1b941295057f140b4
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spelling oai:doaj.org-article:f70b1837e60148e1b941295057f140b42021-11-17T14:21:57ZEffect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry1947-63371947-634510.1080/19476337.2021.1995505https://doaj.org/article/f70b1837e60148e1b941295057f140b42021-01-01T00:00:00Zhttp://dx.doi.org/10.1080/19476337.2021.1995505https://doaj.org/toc/1947-6337https://doaj.org/toc/1947-6345The objective of this research was to evaluate the polyphenolic compounds, the antioxidant activity, and the individual identification of the different types of phenolic compounds in dried extracts of Opuntia atropes. O. atropes extract was dehydrated in a drying oven at 50°C/24 h and by nano-spray drying at 105°C. Drying by nano-spray did not affect the content of phenolic compounds or the antioxidant activity of the O. atropes extract, presenting values of 11.80 ± 0.61 mg of gallic acid equivalent/g of phenolic acids, 22.26 ± 1.02 mg quercetin equivalent/g of flavonoids and inhibition percentage of the radical DPPH• (2,2-. diphenil-1-picrilhidrazil) and ABTS•+ (2,2ʹAzinobis(3-ethylbenzothiazoline-6 sulfonic acid)) of 17.92 ± 0.31 and 54.08 ± 0.48, respectively. In the powdered extracts of O. atropes, glycosides of kaempferol and isorhamnetin were mainly identified by ultra high-performance liquid chromatography coupled to mass spectrometry. Mediorresinol lignan was identified for the first time in this Opuntia species.Eunice Tranquilino-RodríguezHéctor E. Martínez-FloresJosé O. Rodiles-LópezGuillermo C.G. Martínez-AvilaTaylor & Francis Grouparticleopuntia atropesdehydrationnano-spraypolyphenolic profileuplc-q/tof-ms2antioxidant activityNutrition. Foods and food supplyTX341-641Food processing and manufactureTP368-456ENESCyTA - Journal of Food, Vol 19, Iss 1, Pp 805-813 (2021)
institution DOAJ
collection DOAJ
language EN
ES
topic opuntia atropes
dehydration
nano-spray
polyphenolic profile
uplc-q/tof-ms2
antioxidant activity
Nutrition. Foods and food supply
TX341-641
Food processing and manufacture
TP368-456
spellingShingle opuntia atropes
dehydration
nano-spray
polyphenolic profile
uplc-q/tof-ms2
antioxidant activity
Nutrition. Foods and food supply
TX341-641
Food processing and manufacture
TP368-456
Eunice Tranquilino-Rodríguez
Héctor E. Martínez-Flores
José O. Rodiles-López
Guillermo C.G. Martínez-Avila
Effect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry
description The objective of this research was to evaluate the polyphenolic compounds, the antioxidant activity, and the individual identification of the different types of phenolic compounds in dried extracts of Opuntia atropes. O. atropes extract was dehydrated in a drying oven at 50°C/24 h and by nano-spray drying at 105°C. Drying by nano-spray did not affect the content of phenolic compounds or the antioxidant activity of the O. atropes extract, presenting values of 11.80 ± 0.61 mg of gallic acid equivalent/g of phenolic acids, 22.26 ± 1.02 mg quercetin equivalent/g of flavonoids and inhibition percentage of the radical DPPH• (2,2-. diphenil-1-picrilhidrazil) and ABTS•+ (2,2ʹAzinobis(3-ethylbenzothiazoline-6 sulfonic acid)) of 17.92 ± 0.31 and 54.08 ± 0.48, respectively. In the powdered extracts of O. atropes, glycosides of kaempferol and isorhamnetin were mainly identified by ultra high-performance liquid chromatography coupled to mass spectrometry. Mediorresinol lignan was identified for the first time in this Opuntia species.
format article
author Eunice Tranquilino-Rodríguez
Héctor E. Martínez-Flores
José O. Rodiles-López
Guillermo C.G. Martínez-Avila
author_facet Eunice Tranquilino-Rodríguez
Héctor E. Martínez-Flores
José O. Rodiles-López
Guillermo C.G. Martínez-Avila
author_sort Eunice Tranquilino-Rodríguez
title Effect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry
title_short Effect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry
title_full Effect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry
title_fullStr Effect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry
title_full_unstemmed Effect of two dehydration processes on extracts from Opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry
title_sort effect of two dehydration processes on extracts from opuntia atropes and characterization of polyphenolic compounds by ultra high-resolution liquid chromatograph coupled with mass spectrometry
publisher Taylor & Francis Group
publishDate 2021
url https://doaj.org/article/f70b1837e60148e1b941295057f140b4
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