SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O

Inthe present work the synthesis, thermal analysis and structural characterization of Pb2[Fe(CN)6].4H2O are described in orderto obtain mixed oxides with technological properties. The starting materials and the decomposition products were characterized by IR spectroscopy, powder X-ray diffraction (X...

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Autores principales:	GIL,DIEGO MAURICIO, CARBONIO,RAÚL E, GÓMEZ,MARÍA INÉS
Lenguaje:	English
Publicado:	Sociedad Chilena de Química 2010
Materias:	Thermal decomposition Pb2[Fe(CN)6].4H2O, Pb2Fe2O5 crystal structure low temperature synthesis
Acceso en línea:	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072010000200009
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spelling	oai:scielo:S0717-970720100002000092010-09-06SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2OGIL,DIEGO MAURICIOCARBONIO,RAÚL EGÓMEZ,MARÍA INÉS Thermal decomposition Pb2[Fe(CN)6].4H2O, Pb2Fe2O5 crystal structure low temperature synthesis Inthe present work the synthesis, thermal analysis and structural characterization of Pb2[Fe(CN)6].4H2O are described in orderto obtain mixed oxides with technological properties. The starting materials and the decomposition products were characterized by IR spectroscopy, powder X-ray diffraction (XRDP) and scanning electron microscopy (SEM). The crystal structure of Pb2[Fe(CN)6].4H2O has been refined by Rietveld analysis using X- ray powder diffraction data. It Crystallizes in the monoclinic system with space group P2(1)/m and the cell unit parameters are a = 10.9755(2)Å, b = 7.6285(1)Å, c = 8.5696(1) Å y ß = 98.8375(9)°. Pb2Fe2O5 has been obtained by a simple method, the thermal decomposition of Pb2[Fe(CN)6].4H2O at 700 °C in air. Pb2Fe2O5 crystallizes in the tetragonal system with cell unit parameters a = b = 7.80 A, c = 15.82 A. PbO is also obtained.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.55 n.2 20102010-06-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072010000200009en10.4067/S0717-97072010000200009
institution	Scielo Chile
collection	Scielo Chile
language	English
topic	Thermal decomposition Pb2[Fe(CN)6].4H2O, Pb2Fe2O5 crystal structure low temperature synthesis
spellingShingle	Thermal decomposition Pb2[Fe(CN)6].4H2O, Pb2Fe2O5 crystal structure low temperature synthesis GIL,DIEGO MAURICIO CARBONIO,RAÚL E GÓMEZ,MARÍA INÉS SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O
description	Inthe present work the synthesis, thermal analysis and structural characterization of Pb2[Fe(CN)6].4H2O are described in orderto obtain mixed oxides with technological properties. The starting materials and the decomposition products were characterized by IR spectroscopy, powder X-ray diffraction (XRDP) and scanning electron microscopy (SEM). The crystal structure of Pb2[Fe(CN)6].4H2O has been refined by Rietveld analysis using X- ray powder diffraction data. It Crystallizes in the monoclinic system with space group P2(1)/m and the cell unit parameters are a = 10.9755(2)Å, b = 7.6285(1)Å, c = 8.5696(1) Å y ß = 98.8375(9)°. Pb2Fe2O5 has been obtained by a simple method, the thermal decomposition of Pb2[Fe(CN)6].4H2O at 700 °C in air. Pb2Fe2O5 crystallizes in the tetragonal system with cell unit parameters a = b = 7.80 A, c = 15.82 A. PbO is also obtained.
author	GIL,DIEGO MAURICIO CARBONIO,RAÚL E GÓMEZ,MARÍA INÉS
author_facet	GIL,DIEGO MAURICIO CARBONIO,RAÚL E GÓMEZ,MARÍA INÉS
author_sort	GIL,DIEGO MAURICIO
title	SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O
title_short	SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O
title_full	SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O
title_fullStr	SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O
title_full_unstemmed	SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O
title_sort	synthesis of pb2fe2o5 by thermal decomposition of pb2[fe(cn)6].4h2o
publisher	Sociedad Chilena de Química
publishDate	2010
url	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072010000200009
work_keys_str_mv	AT gildiegomauricio synthesisofpb2fe2o5bythermaldecompositionofpb2fecn64h2o AT carbonioraule synthesisofpb2fe2o5bythermaldecompositionofpb2fecn64h2o AT gomezmariaines synthesisofpb2fe2o5bythermaldecompositionofpb2fecn64h2o
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SYNTHESIS OF Pb2Fe2O5 BY THERMAL DECOMPOSITION OF Pb2[Fe(CN)6].4H2O

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