RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12

Zero-strain anode material of Li4Ti5O12 for lithium ion battery was successfully synthesized via the rheological phase reaction (RPR) method. The as-prepared powders were characterized by means of powder X-ray diffraction (XRD), scanning electron microscope (SEM) and particle size distribution analy...

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Autores principales:	XIE,LINGLING, CAO,XIAOYU, LIU,CHANGWEI, WANG,CHIWEI
Lenguaje:	English
Publicado:	Sociedad Chilena de Química 2010
Materias:	rheological phase synthesis characterization Li4Ti5O12 anode material lithium ion batteries
Acceso en línea:	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072010000300015
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spelling	oai:scielo:S0717-970720100003000152011-01-25RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12XIE,LINGLINGCAO,XIAOYULIU,CHANGWEIWANG,CHIWEI rheological phase synthesis characterization Li4Ti5O12 anode material lithium ion batteries Zero-strain anode material of Li4Ti5O12 for lithium ion battery was successfully synthesized via the rheological phase reaction (RPR) method. The as-prepared powders were characterized by means of powder X-ray diffraction (XRD), scanning electron microscope (SEM) and particle size distribution analysis (PSD), and the electrochemical properties of the powders were evaluated by the galvanostatic discharge test and cyclic voltammetry (CV). The results revealed that well-crystallized uniform micro-sized Li4Ti5O12 powders were obtained at 800°C for different calcination times via the simple template-free rheological phase route. Among these RPR-derived Li4Ti5O12 powders, one synthesized at 800°C for 22 h displays the initial discharge capacity of 184.3 mAh/g and excellent characteristic of cyclic voltammetry.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.55 n.3 20102010-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072010000300015en10.4067/S0717-97072010000300015
institution	Scielo Chile
collection	Scielo Chile
language	English
topic	rheological phase synthesis characterization Li4Ti5O12 anode material lithium ion batteries
spellingShingle	rheological phase synthesis characterization Li4Ti5O12 anode material lithium ion batteries XIE,LINGLING CAO,XIAOYU LIU,CHANGWEI WANG,CHIWEI RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12
description	Zero-strain anode material of Li4Ti5O12 for lithium ion battery was successfully synthesized via the rheological phase reaction (RPR) method. The as-prepared powders were characterized by means of powder X-ray diffraction (XRD), scanning electron microscope (SEM) and particle size distribution analysis (PSD), and the electrochemical properties of the powders were evaluated by the galvanostatic discharge test and cyclic voltammetry (CV). The results revealed that well-crystallized uniform micro-sized Li4Ti5O12 powders were obtained at 800°C for different calcination times via the simple template-free rheological phase route. Among these RPR-derived Li4Ti5O12 powders, one synthesized at 800°C for 22 h displays the initial discharge capacity of 184.3 mAh/g and excellent characteristic of cyclic voltammetry.
author	XIE,LINGLING CAO,XIAOYU LIU,CHANGWEI WANG,CHIWEI
author_facet	XIE,LINGLING CAO,XIAOYU LIU,CHANGWEI WANG,CHIWEI
author_sort	XIE,LINGLING
title	RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12
title_short	RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12
title_full	RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12
title_fullStr	RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12
title_full_unstemmed	RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12
title_sort	rheological phase synthesis and characterization of micro-sized li4ti5o12
publisher	Sociedad Chilena de Química
publishDate	2010
url	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072010000300015
work_keys_str_mv	AT xielingling rheologicalphasesynthesisandcharacterizationofmicrosizedli4ti5o12 AT caoxiaoyu rheologicalphasesynthesisandcharacterizationofmicrosizedli4ti5o12 AT liuchangwei rheologicalphasesynthesisandcharacterizationofmicrosizedli4ti5o12 AT wangchiwei rheologicalphasesynthesisandcharacterizationofmicrosizedli4ti5o12
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RHEOLOGICAL PHASE SYNTHESIS AND CHARACTERIZATION OF MICRO-SIZED Li4Ti5O12

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