PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION

A new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. Eight nano-baskets of p-tert-calix[4]arene bearing di-[N-(X)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were...

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Autores principales: MOKHTARI,BAHRAM, POURABDOLLAH,KOBRA
Lenguaje:English
Publicado: Sociedad Chilena de Química 2012
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Acceso en línea:http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000200020
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spelling oai:scielo:S0717-970720120002000202014-03-10PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATIONMOKHTARI,BAHRAMPOURABDOLLAH,KOBRA Bonded-Phase Partial-Cone Conformation Calixarene Salbutamol nanobasket A new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. Eight nano-baskets of p-tert-calix[4]arene bearing di-[N-(X)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were used to prepare bended phases of HPLC-UV. The new synthesized bonded-phases were characterized and optimized, the bonding interactions of solute and stationary phases were examined and the main interactions were reported. The results revealed that for the best bonded-phase, the LOD and LOQ were 0.02 and 0.06 μg/mL, respectively.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.57 n.2 20122012-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000200020en10.4067/S0717-97072012000200020
institution Scielo Chile
collection Scielo Chile
language English
topic Bonded-Phase
Partial-Cone Conformation
Calixarene
Salbutamol
nanobasket
spellingShingle Bonded-Phase
Partial-Cone Conformation
Calixarene
Salbutamol
nanobasket
MOKHTARI,BAHRAM
POURABDOLLAH,KOBRA
PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
description A new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. Eight nano-baskets of p-tert-calix[4]arene bearing di-[N-(X)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were used to prepare bended phases of HPLC-UV. The new synthesized bonded-phases were characterized and optimized, the bonding interactions of solute and stationary phases were examined and the main interactions were reported. The results revealed that for the best bonded-phase, the LOD and LOQ were 0.02 and 0.06 μg/mL, respectively.
author MOKHTARI,BAHRAM
POURABDOLLAH,KOBRA
author_facet MOKHTARI,BAHRAM
POURABDOLLAH,KOBRA
author_sort MOKHTARI,BAHRAM
title PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
title_short PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
title_full PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
title_fullStr PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
title_full_unstemmed PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
title_sort preparation and characterization of bonded-phases of calixarene-sulfonyl-carboxamides in partial-cone conformation for determination of salbutamol in livestock by nano-mediated bonded-phases: nano-baskets of calixarene in partial-cone conformation
publisher Sociedad Chilena de Química
publishDate 2012
url http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000200020
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