PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
A new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. Eight nano-baskets of p-tert-calix[4]arene bearing di-[N-(X)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were...
Guardado en:
Autores principales: | , |
---|---|
Lenguaje: | English |
Publicado: |
Sociedad Chilena de Química
2012
|
Materias: | |
Acceso en línea: | http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000200020 |
Etiquetas: |
Agregar Etiqueta
Sin Etiquetas, Sea el primero en etiquetar este registro!
|
id |
oai:scielo:S0717-97072012000200020 |
---|---|
record_format |
dspace |
spelling |
oai:scielo:S0717-970720120002000202014-03-10PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATIONMOKHTARI,BAHRAMPOURABDOLLAH,KOBRA Bonded-Phase Partial-Cone Conformation Calixarene Salbutamol nanobasket A new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. Eight nano-baskets of p-tert-calix[4]arene bearing di-[N-(X)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were used to prepare bended phases of HPLC-UV. The new synthesized bonded-phases were characterized and optimized, the bonding interactions of solute and stationary phases were examined and the main interactions were reported. The results revealed that for the best bonded-phase, the LOD and LOQ were 0.02 and 0.06 μg/mL, respectively.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.57 n.2 20122012-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000200020en10.4067/S0717-97072012000200020 |
institution |
Scielo Chile |
collection |
Scielo Chile |
language |
English |
topic |
Bonded-Phase Partial-Cone Conformation Calixarene Salbutamol nanobasket |
spellingShingle |
Bonded-Phase Partial-Cone Conformation Calixarene Salbutamol nanobasket MOKHTARI,BAHRAM POURABDOLLAH,KOBRA PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION |
description |
A new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. Eight nano-baskets of p-tert-calix[4]arene bearing di-[N-(X)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were used to prepare bended phases of HPLC-UV. The new synthesized bonded-phases were characterized and optimized, the bonding interactions of solute and stationary phases were examined and the main interactions were reported. The results revealed that for the best bonded-phase, the LOD and LOQ were 0.02 and 0.06 μg/mL, respectively. |
author |
MOKHTARI,BAHRAM POURABDOLLAH,KOBRA |
author_facet |
MOKHTARI,BAHRAM POURABDOLLAH,KOBRA |
author_sort |
MOKHTARI,BAHRAM |
title |
PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION |
title_short |
PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION |
title_full |
PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION |
title_fullStr |
PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION |
title_full_unstemmed |
PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION |
title_sort |
preparation and characterization of bonded-phases of calixarene-sulfonyl-carboxamides in partial-cone conformation for determination of salbutamol in livestock by nano-mediated bonded-phases: nano-baskets of calixarene in partial-cone conformation |
publisher |
Sociedad Chilena de Química |
publishDate |
2012 |
url |
http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000200020 |
work_keys_str_mv |
AT mokhtaribahram preparationandcharacterizationofbondedphasesofcalixarenesulfonylcarboxamidesinpartialconeconformationfordeterminationofsalbutamolinlivestockbynanomediatedbondedphasesnanobasketsofcalixareneinpartialconeconformation AT pourabdollahkobra preparationandcharacterizationofbondedphasesofcalixarenesulfonylcarboxamidesinpartialconeconformationfordeterminationofsalbutamolinlivestockbynanomediatedbondedphasesnanobasketsofcalixareneinpartialconeconformation |
_version_ |
1718445466059800576 |