CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS

The essential oils obtained by hydrodistillation from samples of propolis manufactured in three regions of Rio Grande do Sul State at Brazil, were analyzed through CG, CG-MS and chiral phase gas chromatography (CPGC). These analyses display the presence of samples with elevated essential oil purport...

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Autores principales: SIMIONATTO,EUCLÉSIO, FACCO,JANAINA T, MOREL,ADEMIR F, GIACOMELLI,SANDRO R, LINARES,CARLOS E. B
Lenguaje:English
Publicado: Sociedad Chilena de Química 2012
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Acceso en línea:http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000300009
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spelling oai:scielo:S0717-970720120003000092019-02-19CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLISSIMIONATTO,EUCLÉSIOFACCO,JANAINA TMOREL,ADEMIR FGIACOMELLI,SANDRO RLINARES,CARLOS E. B propolis essential oil chiral phase gas chromatography enantiomeric composition antimicrobial activity The essential oils obtained by hydrodistillation from samples of propolis manufactured in three regions of Rio Grande do Sul State at Brazil, were analyzed through CG, CG-MS and chiral phase gas chromatography (CPGC). These analyses display the presence of samples with elevated essential oil purport, when compared with plants. The yields obtained were until 3.8%. The samples exhibited similar composition, with predominance of the monoterpenes α-pinene (5763%), β-pinene (12.5-30.8%) and limonene (1.5-11.2%). In chiral analysis ofthese constituents were observed modifications in the enantiomeric excess of isomers of α-pinene and limonene in relation with source location of the sample, already in the chiral analysis of β-pinene were detected only elevated excess of the enantiomer with the (-) configuration. The antimicrobial activity of the crude essential oil was assayed against five bacteria. The best result was obtained against Staphylococcus aureus.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.57 n.3 20122012-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000300009en10.4067/S0717-97072012000300009
institution Scielo Chile
collection Scielo Chile
language English
topic propolis
essential oil
chiral phase gas chromatography
enantiomeric composition
antimicrobial activity
spellingShingle propolis
essential oil
chiral phase gas chromatography
enantiomeric composition
antimicrobial activity
SIMIONATTO,EUCLÉSIO
FACCO,JANAINA T
MOREL,ADEMIR F
GIACOMELLI,SANDRO R
LINARES,CARLOS E. B
CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS
description The essential oils obtained by hydrodistillation from samples of propolis manufactured in three regions of Rio Grande do Sul State at Brazil, were analyzed through CG, CG-MS and chiral phase gas chromatography (CPGC). These analyses display the presence of samples with elevated essential oil purport, when compared with plants. The yields obtained were until 3.8%. The samples exhibited similar composition, with predominance of the monoterpenes α-pinene (5763%), β-pinene (12.5-30.8%) and limonene (1.5-11.2%). In chiral analysis ofthese constituents were observed modifications in the enantiomeric excess of isomers of α-pinene and limonene in relation with source location of the sample, already in the chiral analysis of β-pinene were detected only elevated excess of the enantiomer with the (-) configuration. The antimicrobial activity of the crude essential oil was assayed against five bacteria. The best result was obtained against Staphylococcus aureus.
author SIMIONATTO,EUCLÉSIO
FACCO,JANAINA T
MOREL,ADEMIR F
GIACOMELLI,SANDRO R
LINARES,CARLOS E. B
author_facet SIMIONATTO,EUCLÉSIO
FACCO,JANAINA T
MOREL,ADEMIR F
GIACOMELLI,SANDRO R
LINARES,CARLOS E. B
author_sort SIMIONATTO,EUCLÉSIO
title CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS
title_short CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS
title_full CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS
title_fullStr CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS
title_full_unstemmed CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS
title_sort chiral analysis of monoterpenes in volatile oils from propolis
publisher Sociedad Chilena de Química
publishDate 2012
url http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000300009
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