CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS
The essential oils obtained by hydrodistillation from samples of propolis manufactured in three regions of Rio Grande do Sul State at Brazil, were analyzed through CG, CG-MS and chiral phase gas chromatography (CPGC). These analyses display the presence of samples with elevated essential oil purport...
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Sociedad Chilena de Química
2012
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oai:scielo:S0717-970720120003000092019-02-19CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLISSIMIONATTO,EUCLÉSIOFACCO,JANAINA TMOREL,ADEMIR FGIACOMELLI,SANDRO RLINARES,CARLOS E. B propolis essential oil chiral phase gas chromatography enantiomeric composition antimicrobial activity The essential oils obtained by hydrodistillation from samples of propolis manufactured in three regions of Rio Grande do Sul State at Brazil, were analyzed through CG, CG-MS and chiral phase gas chromatography (CPGC). These analyses display the presence of samples with elevated essential oil purport, when compared with plants. The yields obtained were until 3.8%. The samples exhibited similar composition, with predominance of the monoterpenes α-pinene (5763%), β-pinene (12.5-30.8%) and limonene (1.5-11.2%). In chiral analysis ofthese constituents were observed modifications in the enantiomeric excess of isomers of α-pinene and limonene in relation with source location of the sample, already in the chiral analysis of β-pinene were detected only elevated excess of the enantiomer with the (-) configuration. The antimicrobial activity of the crude essential oil was assayed against five bacteria. The best result was obtained against Staphylococcus aureus.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.57 n.3 20122012-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000300009en10.4067/S0717-97072012000300009 |
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Scielo Chile |
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Scielo Chile |
language |
English |
topic |
propolis essential oil chiral phase gas chromatography enantiomeric composition antimicrobial activity |
spellingShingle |
propolis essential oil chiral phase gas chromatography enantiomeric composition antimicrobial activity SIMIONATTO,EUCLÉSIO FACCO,JANAINA T MOREL,ADEMIR F GIACOMELLI,SANDRO R LINARES,CARLOS E. B CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS |
description |
The essential oils obtained by hydrodistillation from samples of propolis manufactured in three regions of Rio Grande do Sul State at Brazil, were analyzed through CG, CG-MS and chiral phase gas chromatography (CPGC). These analyses display the presence of samples with elevated essential oil purport, when compared with plants. The yields obtained were until 3.8%. The samples exhibited similar composition, with predominance of the monoterpenes α-pinene (5763%), β-pinene (12.5-30.8%) and limonene (1.5-11.2%). In chiral analysis ofthese constituents were observed modifications in the enantiomeric excess of isomers of α-pinene and limonene in relation with source location of the sample, already in the chiral analysis of β-pinene were detected only elevated excess of the enantiomer with the (-) configuration. The antimicrobial activity of the crude essential oil was assayed against five bacteria. The best result was obtained against Staphylococcus aureus. |
author |
SIMIONATTO,EUCLÉSIO FACCO,JANAINA T MOREL,ADEMIR F GIACOMELLI,SANDRO R LINARES,CARLOS E. B |
author_facet |
SIMIONATTO,EUCLÉSIO FACCO,JANAINA T MOREL,ADEMIR F GIACOMELLI,SANDRO R LINARES,CARLOS E. B |
author_sort |
SIMIONATTO,EUCLÉSIO |
title |
CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS |
title_short |
CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS |
title_full |
CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS |
title_fullStr |
CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS |
title_full_unstemmed |
CHIRAL ANALYSIS OF MONOTERPENES IN VOLATILE OILS FROM PROPOLIS |
title_sort |
chiral analysis of monoterpenes in volatile oils from propolis |
publisher |
Sociedad Chilena de Química |
publishDate |
2012 |
url |
http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072012000300009 |
work_keys_str_mv |
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