CRYSTAL STRUCTURE OF A PERINDOPRIL CYCLIZATION PRODUCT, C19H30N2O4

CRYSTAL STRUCTURE OF A PERINDOPRIL CYCLIZATION PRODUCT, C19H30N2O4

The title compound is a product of perindopril intramolecular cyclization. It crystallizes in the tetragonal, non-centrosymmetric space group P4(1)2(1)2 (No. 92) with a = 9.3574(2), b = 9.3574(2), c = 45.6369(9) Å, V = 3996.01(14) ų and Z = 8. The crystal consists of one molecule in the asymmetric...

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Detalles Bibliográficos
Autores principales: BOJARSKA,JOANNA, MANIUKIEWICZ,WALDEMAR, GLÓWKA,MAREK L, SIERÓN,LESLAW, REMKO,MILAN
Lenguaje:English
Publicado: Sociedad Chilena de Química 2013
Materias:
crystal structure
X-ray diffraction
perindopril
Acceso en línea:http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072013000100006
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Sumario:The title compound is a product of perindopril intramolecular cyclization. It crystallizes in the tetragonal, non-centrosymmetric space group P4(1)2(1)2 (No. 92) with a = 9.3574(2), b = 9.3574(2), c = 45.6369(9) Å, V = 3996.01(14) ų and Z = 8. The crystal consists of one molecule in the asymmetric unit. The packing exhibits weak intermolecular C-H - O=C contacts forming two C(5) and C(10) chains, which together result in graph-set descriptor R³3 (18) motif, running along the crystallographic a-axis.

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