VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY

A rapid, specific and sensitive multi-residue method based on the quick, east, cheap, effective, rugged and safe (QuEChERS) has been developed and validated for the determination of 19 multi-class insecticide and fungicide residues (Aldrin, Amitraz, Bromopropylate, Chlorpyrifos, DDT, Diazinon, Dichl...

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Autores principales:	DASHTBOZORGI,ZAHRA, RAMEZANI,MOHAMMAD KAZEM, HUSAIN,SYED WAQIF, ABRUMAND-AZAR,PARVIZ, MOROWATI,MOHSEN
Lenguaje:	English
Publicado:	Sociedad Chilena de Química 2013
Materias:	QuEChERS Pesticide residues Matrix matched calibration Insecticides Fungicides GC/MS-SIM
Acceso en línea:	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072013000200012
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spelling	oai:scielo:S0717-970720130002000122014-09-09VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRYDASHTBOZORGI,ZAHRARAMEZANI,MOHAMMAD KAZEMHUSAIN,SYED WAQIFABRUMAND-AZAR,PARVIZMOROWATI,MOHSEN QuEChERS Pesticide residues Matrix matched calibration Insecticides Fungicides GC/MS-SIM A rapid, specific and sensitive multi-residue method based on the quick, east, cheap, effective, rugged and safe (QuEChERS) has been developed and validated for the determination of 19 multi-class insecticide and fungicide residues (Aldrin, Amitraz, Bromopropylate, Chlorpyrifos, DDT, Diazinon, Dichlorovos, Ethion, Fenpropathrin, Fenvalerate, Iprodion, Malathion, Metalaxyl, Oxydemethon methyl, Permethrin, Phosalone, Pirimicarb, Profenofos and Tetradifon) in greenhouse cucumber and tomato. Gas chromatography-mass spectrometric detection in selected ion monitoring mode (GC/MS-SIM) was applied for determination of pesticides residues. Quantification was performed using matrix-matched calibration and solvent calibration. Recovery studies were used for comparison of accuracy of each calibration method. Results showed matrix matched calibration would be efficient for quantification of pesticide residues in Iranian cucumber and tomato.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.58 n.2 20132013-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072013000200012en10.4067/S0717-97072013000200012
institution	Scielo Chile
collection	Scielo Chile
language	English
topic	QuEChERS Pesticide residues Matrix matched calibration Insecticides Fungicides GC/MS-SIM
spellingShingle	QuEChERS Pesticide residues Matrix matched calibration Insecticides Fungicides GC/MS-SIM DASHTBOZORGI,ZAHRA RAMEZANI,MOHAMMAD KAZEM HUSAIN,SYED WAQIF ABRUMAND-AZAR,PARVIZ MOROWATI,MOHSEN VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY
description	A rapid, specific and sensitive multi-residue method based on the quick, east, cheap, effective, rugged and safe (QuEChERS) has been developed and validated for the determination of 19 multi-class insecticide and fungicide residues (Aldrin, Amitraz, Bromopropylate, Chlorpyrifos, DDT, Diazinon, Dichlorovos, Ethion, Fenpropathrin, Fenvalerate, Iprodion, Malathion, Metalaxyl, Oxydemethon methyl, Permethrin, Phosalone, Pirimicarb, Profenofos and Tetradifon) in greenhouse cucumber and tomato. Gas chromatography-mass spectrometric detection in selected ion monitoring mode (GC/MS-SIM) was applied for determination of pesticides residues. Quantification was performed using matrix-matched calibration and solvent calibration. Recovery studies were used for comparison of accuracy of each calibration method. Results showed matrix matched calibration would be efficient for quantification of pesticide residues in Iranian cucumber and tomato.
author	DASHTBOZORGI,ZAHRA RAMEZANI,MOHAMMAD KAZEM HUSAIN,SYED WAQIF ABRUMAND-AZAR,PARVIZ MOROWATI,MOHSEN
author_facet	DASHTBOZORGI,ZAHRA RAMEZANI,MOHAMMAD KAZEM HUSAIN,SYED WAQIF ABRUMAND-AZAR,PARVIZ MOROWATI,MOHSEN
author_sort	DASHTBOZORGI,ZAHRA
title	VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY
title_short	VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY
title_full	VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY
title_fullStr	VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY
title_full_unstemmed	VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY
title_sort	validation of matrix matched calibration for analysis of insecticide and fungicid residues in cucumber and tomato using quechers sample preparation followed by gas chromatography-mass spectrometry
publisher	Sociedad Chilena de Química
publishDate	2013
url	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072013000200012
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VALIDATION OF MATRIX MATCHED CALIBRATION FOR ANALYSIS OF INSECTICIDE AND FUNGICID RESIDUES IN CUCUMBER AND TOMATO USING QuEChERS SAMPLE PREPARATION FOLLOWED BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY

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