SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES

SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES

In the present study 1, 5-benzodiazepines were synthesized from a range of α, β-unsaturated ketones and o-phenylendiamine using oxalic acid 10 mol% as a catalyst under solvent free conditions. The yields of the present method are better than the reported method which explains effec...

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Autores principales: SARKATE,ANIKET P, SANGSHETTI,JAIPRAKASH N, DHARBALE,NANASAHEB B, SARKATE,AJINKYA P, WAKTE,PRAVIN S, SHINDE,DEVANAND B
Lenguaje:English
Publicado: Sociedad Chilena de Química 2013
Materias:
1, 5-benzodiazepine
oxalic acid
solvent free conditions
α, β-unsaturated ketones
o-phenylenediamine
Acceso en línea:http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072013000400064
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spelling oai:scielo:S0717-970720130004000642014-09-02SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINESSARKATE,ANIKET PSANGSHETTI,JAIPRAKASH NDHARBALE,NANASAHEB BSARKATE,AJINKYA PWAKTE,PRAVIN SSHINDE,DEVANAND B 1, 5-benzodiazepine oxalic acid solvent free conditions α, β-unsaturated ketones o-phenylenediamine In the present study 1, 5-benzodiazepines were synthesized from a range of α, β-unsaturated ketones and o-phenylendiamine using oxalic acid 10 mol% as a catalyst under solvent free conditions. The yields of the present method are better than the reported method which explains effectiveness of oxalic acid catalyst. The cost effective, resourceful, undemanding and environment friendly are the advantageous aspects of this method.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.58 n.4 20132013-12-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072013000400064en10.4067/S0717-97072013000400064
institution Scielo Chile
collection Scielo Chile
language English
topic 1, 5-benzodiazepine
oxalic acid
solvent free conditions
α, β-unsaturated ketones
o-phenylenediamine
spellingShingle 1, 5-benzodiazepine
oxalic acid
solvent free conditions
α, β-unsaturated ketones
o-phenylenediamine
SARKATE,ANIKET P
SANGSHETTI,JAIPRAKASH N
DHARBALE,NANASAHEB B
SARKATE,AJINKYA P
WAKTE,PRAVIN S
SHINDE,DEVANAND B
SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES
description In the present study 1, 5-benzodiazepines were synthesized from a range of α, β-unsaturated ketones and o-phenylendiamine using oxalic acid 10 mol% as a catalyst under solvent free conditions. The yields of the present method are better than the reported method which explains effectiveness of oxalic acid catalyst. The cost effective, resourceful, undemanding and environment friendly are the advantageous aspects of this method.
author SARKATE,ANIKET P
SANGSHETTI,JAIPRAKASH N
DHARBALE,NANASAHEB B
SARKATE,AJINKYA P
WAKTE,PRAVIN S
SHINDE,DEVANAND B
author_facet SARKATE,ANIKET P
SANGSHETTI,JAIPRAKASH N
DHARBALE,NANASAHEB B
SARKATE,AJINKYA P
WAKTE,PRAVIN S
SHINDE,DEVANAND B
author_sort SARKATE,ANIKET P
title SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES
title_short SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES
title_full SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES
title_fullStr SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES
title_full_unstemmed SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES
title_sort solvent free oxalic acid catalyzed synthesis of 1,5-benzodiazepines
publisher Sociedad Chilena de Química
publishDate 2013
url http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072013000400064
work_keys_str_mv AT sarkateaniketp solventfreeoxalicacidcatalyzedsynthesisof15benzodiazepines
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AT dharbalenanasahebb solventfreeoxalicacidcatalyzedsynthesisof15benzodiazepines
AT sarkateajinkyap solventfreeoxalicacidcatalyzedsynthesisof15benzodiazepines
AT waktepravins solventfreeoxalicacidcatalyzedsynthesisof15benzodiazepines
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