MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERING
Gold nanoparticles (AuNPs) were deposited by DC-magnetron sputtering onto molybdenum trioxide (MoO3) thin films grown by Photochemical Metal-Organic Deposition (PMOD) on Si(100) and borosilicate glass substrates. The chemical, optical and morphology properties of the films were studied by UV/ Vis Sp...
Guardado en:
Autores principales: | , , , , , , |
---|---|
Lenguaje: | English |
Publicado: |
Sociedad Chilena de Química
2016
|
Materias: | |
Acceso en línea: | http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072016000100014 |
Etiquetas: |
Agregar Etiqueta
Sin Etiquetas, Sea el primero en etiquetar este registro!
|
id |
oai:scielo:S0717-97072016000100014 |
---|---|
record_format |
dspace |
spelling |
oai:scielo:S0717-970720160001000142016-09-14MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERINGCASTILLO,CBUONO-CORE,GMANZUR,CYUTRONIC,NSIERPE,RCABELLO,GCHORNIK,B A. oxides A. thin films A. nanostructures B. sputtering C. x-ray diffraction C. photoelectron spectroscopy Gold nanoparticles (AuNPs) were deposited by DC-magnetron sputtering onto molybdenum trioxide (MoO3) thin films grown by Photochemical Metal-Organic Deposition (PMOD) on Si(100) and borosilicate glass substrates. The chemical, optical and morphology properties of the films were studied by UV/ Vis Spectroscopy, Scanning Electron Microscopy (SEM), X-Ray Photoelectron Spectroscopy (XPS), and X-Ray Diffraction (XRD). SEM revealed that AuNPs formed after 5 s of sputtering. AuNPs are spherical and have both an average diameter of 18 nm and a relatively narrow size distribution. As the deposition time increases, larger structures are formed by an aggregation of AuNPs. XPS studies of the AuNP/MoO3 films on Si(100) showed the presence of Mo(VI) and Mo(V), which indicated that the films were primarily non-stoichiometric molybdenum oxides. The occurrence of oxygen vacancies in the substrate play an important role to stabilize the AuNPs.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.61 n.1 20162016-03-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072016000100014en10.4067/S0717-97072016000100014 |
institution |
Scielo Chile |
collection |
Scielo Chile |
language |
English |
topic |
A. oxides A. thin films A. nanostructures B. sputtering C. x-ray diffraction C. photoelectron spectroscopy |
spellingShingle |
A. oxides A. thin films A. nanostructures B. sputtering C. x-ray diffraction C. photoelectron spectroscopy CASTILLO,C BUONO-CORE,G MANZUR,C YUTRONIC,N SIERPE,R CABELLO,G CHORNIK,B MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERING |
description |
Gold nanoparticles (AuNPs) were deposited by DC-magnetron sputtering onto molybdenum trioxide (MoO3) thin films grown by Photochemical Metal-Organic Deposition (PMOD) on Si(100) and borosilicate glass substrates. The chemical, optical and morphology properties of the films were studied by UV/ Vis Spectroscopy, Scanning Electron Microscopy (SEM), X-Ray Photoelectron Spectroscopy (XPS), and X-Ray Diffraction (XRD). SEM revealed that AuNPs formed after 5 s of sputtering. AuNPs are spherical and have both an average diameter of 18 nm and a relatively narrow size distribution. As the deposition time increases, larger structures are formed by an aggregation of AuNPs. XPS studies of the AuNP/MoO3 films on Si(100) showed the presence of Mo(VI) and Mo(V), which indicated that the films were primarily non-stoichiometric molybdenum oxides. The occurrence of oxygen vacancies in the substrate play an important role to stabilize the AuNPs. |
author |
CASTILLO,C BUONO-CORE,G MANZUR,C YUTRONIC,N SIERPE,R CABELLO,G CHORNIK,B |
author_facet |
CASTILLO,C BUONO-CORE,G MANZUR,C YUTRONIC,N SIERPE,R CABELLO,G CHORNIK,B |
author_sort |
CASTILLO,C |
title |
MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERING |
title_short |
MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERING |
title_full |
MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERING |
title_fullStr |
MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERING |
title_full_unstemmed |
MOLYBDENUM TRIOXIDE THIN FILMS DOPED WITH GOLD NANOPARTICLES GROWN BY A SEQUENTIAL METHODOLOGY: PHOTOCHEMICAL METAL-ORGANIC DEPOSITION (PMOD) AND DC-MAGNETRON SPUTTERING |
title_sort |
molybdenum trioxide thin films doped with gold nanoparticles grown by a sequential methodology: photochemical metal-organic deposition (pmod) and dc-magnetron sputtering |
publisher |
Sociedad Chilena de Química |
publishDate |
2016 |
url |
http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072016000100014 |
work_keys_str_mv |
AT castilloc molybdenumtrioxidethinfilmsdopedwithgoldnanoparticlesgrownbyasequentialmethodologyphotochemicalmetalorganicdepositionpmodanddcmagnetronsputtering AT buonocoreg molybdenumtrioxidethinfilmsdopedwithgoldnanoparticlesgrownbyasequentialmethodologyphotochemicalmetalorganicdepositionpmodanddcmagnetronsputtering AT manzurc molybdenumtrioxidethinfilmsdopedwithgoldnanoparticlesgrownbyasequentialmethodologyphotochemicalmetalorganicdepositionpmodanddcmagnetronsputtering AT yutronicn molybdenumtrioxidethinfilmsdopedwithgoldnanoparticlesgrownbyasequentialmethodologyphotochemicalmetalorganicdepositionpmodanddcmagnetronsputtering AT sierper molybdenumtrioxidethinfilmsdopedwithgoldnanoparticlesgrownbyasequentialmethodologyphotochemicalmetalorganicdepositionpmodanddcmagnetronsputtering AT cabellog molybdenumtrioxidethinfilmsdopedwithgoldnanoparticlesgrownbyasequentialmethodologyphotochemicalmetalorganicdepositionpmodanddcmagnetronsputtering AT chornikb molybdenumtrioxidethinfilmsdopedwithgoldnanoparticlesgrownbyasequentialmethodologyphotochemicalmetalorganicdepositionpmodanddcmagnetronsputtering |
_version_ |
1718445548200001536 |