ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS

Nano-TiCl4.SiO2 has been introduced to be an extremely efficient catalyst for the preparation of N,N'-alkylidene bisamides from various aldehydes and amides under mild conditions. We synthesized this solid Lewis acid catalyst by the reaction of nano-SiO2 and TiCl4. The processor was simple and...

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Autores principales:	KHABNADIDEH,SOGHRA, ZOMORODIAN,KAMIAR, MIRJALILI,BI BI FATEMEH, IZADI,ELHAM, ZAMANI,LEILA
Lenguaje:	English
Publicado:	Sociedad Chilena de Química 2016
Materias:	Nano-TiCl4.SiO2 Heterogeneous catalyst N,N'-Alkylidene bisamides Antifungal Antibacterial
Acceso en línea:	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072016000300005
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spelling	oai:scielo:S0717-970720160003000052017-06-14ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTSKHABNADIDEH,SOGHRAZOMORODIAN,KAMIARMIRJALILI,BI BI FATEMEHIZADI,ELHAMZAMANI,LEILA Nano-TiCl4.SiO2 Heterogeneous catalyst N,N'-Alkylidene bisamides Antifungal Antibacterial Nano-TiCl4.SiO2 has been introduced to be an extremely efficient catalyst for the preparation of N,N'-alkylidene bisamides from various aldehydes and amides under mild conditions. We synthesized this solid Lewis acid catalyst by the reaction of nano-SiO2 and TiCl4. The processor was simple and environmentally benign with high to excellent yields. Our method has the advantages of high yields, simple methodology, and easy work-up. The antimicrobial and antifungal activities of some of the synthetic compounds were determined by broth microdilution methods as recommended by Clinical Laboratory Standard Institute. Further studies still needed to investigate the other biological activities of the compounds.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.61 n.3 20162016-09-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072016000300005en10.4067/S0717-97072016000300005
institution	Scielo Chile
collection	Scielo Chile
language	English
topic	Nano-TiCl4.SiO2 Heterogeneous catalyst N,N'-Alkylidene bisamides Antifungal Antibacterial
spellingShingle	Nano-TiCl4.SiO2 Heterogeneous catalyst N,N'-Alkylidene bisamides Antifungal Antibacterial KHABNADIDEH,SOGHRA ZOMORODIAN,KAMIAR MIRJALILI,BI BI FATEMEH IZADI,ELHAM ZAMANI,LEILA ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS
description	Nano-TiCl4.SiO2 has been introduced to be an extremely efficient catalyst for the preparation of N,N'-alkylidene bisamides from various aldehydes and amides under mild conditions. We synthesized this solid Lewis acid catalyst by the reaction of nano-SiO2 and TiCl4. The processor was simple and environmentally benign with high to excellent yields. Our method has the advantages of high yields, simple methodology, and easy work-up. The antimicrobial and antifungal activities of some of the synthetic compounds were determined by broth microdilution methods as recommended by Clinical Laboratory Standard Institute. Further studies still needed to investigate the other biological activities of the compounds.
author	KHABNADIDEH,SOGHRA ZOMORODIAN,KAMIAR MIRJALILI,BI BI FATEMEH IZADI,ELHAM ZAMANI,LEILA
author_facet	KHABNADIDEH,SOGHRA ZOMORODIAN,KAMIAR MIRJALILI,BI BI FATEMEH IZADI,ELHAM ZAMANI,LEILA
author_sort	KHABNADIDEH,SOGHRA
title	ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS
title_short	ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS
title_full	ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS
title_fullStr	ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS
title_full_unstemmed	ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS
title_sort	one pot preparations n,n'-alkylidene bisamide derivatives catalyzed by nano-ticl4.sio2 with antimicrobial studies of some products
publisher	Sociedad Chilena de Química
publishDate	2016
url	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072016000300005
work_keys_str_mv	AT khabnadidehsoghra onepotpreparationsnnalkylidenebisamidederivativescatalyzedbynanoticl4sio2withantimicrobialstudiesofsomeproducts AT zomorodiankamiar onepotpreparationsnnalkylidenebisamidederivativescatalyzedbynanoticl4sio2withantimicrobialstudiesofsomeproducts AT mirjalilibibifatemeh onepotpreparationsnnalkylidenebisamidederivativescatalyzedbynanoticl4sio2withantimicrobialstudiesofsomeproducts AT izadielham onepotpreparationsnnalkylidenebisamidederivativescatalyzedbynanoticl4sio2withantimicrobialstudiesofsomeproducts AT zamanileila onepotpreparationsnnalkylidenebisamidederivativescatalyzedbynanoticl4sio2withantimicrobialstudiesofsomeproducts
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ONE POT PREPARATIONS N,N'-ALKYLIDENE BISAMIDE DERIVATIVES CATALYZED BY NANO-TiCL4.SiO2 WITH ANTIMICROBIAL STUDIES OF SOME PRODUCTS

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