SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)

ABSTRACT In this study, we examined the synthesis, and characterization of TiO2/poly(N-maleoylglycine-co-acrylic acid) (TiO2/poly(MG-co-AA)) nanocomposite. The nanocomposite was prepared by the dispersion of TiO2 nanotubes in a water solution of the polymer (3% w/w) and then it was lyophilized. The...

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Autores principales:	OYARZÚN,DIEGO P., PIZARRO,GUADALUPE DEL C., ASENJO,ANDRÉS, TELLO,ALEJANDRA, MARTIN-TRASANCO,RUDY, ZÚÑIGA,CÉSAR, SÁNCHEZ,JULIO, ARRATIA-PEREZ,RAMIRO
Lenguaje:	English
Publicado:	Sociedad Chilena de Química 2017
Materias:	polymer nanocomposite morphological characterization TiO2 nanotubes
Acceso en línea:	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072017000303634
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spelling	oai:scielo:S0717-970720170003036342017-09-08SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)OYARZÚN,DIEGO P.PIZARRO,GUADALUPE DEL C.ASENJO,ANDRÉSTELLO,ALEJANDRAMARTIN-TRASANCO,RUDYZÚÑIGA,CÉSARSÁNCHEZ,JULIOARRATIA-PEREZ,RAMIRO polymer nanocomposite morphological characterization TiO2 nanotubes ABSTRACT In this study, we examined the synthesis, and characterization of TiO2/poly(N-maleoylglycine-co-acrylic acid) (TiO2/poly(MG-co-AA)) nanocomposite. The nanocomposite was prepared by the dispersion of TiO2 nanotubes in a water solution of the polymer (3% w/w) and then it was lyophilized. The nanocomposite was characterized by FTIR and Raman spectroscopies. The incorporation of TiO2 nanotubes to the polymeric matrix was determined by transmission electron microscopy (TEM) from which TiO2 nanotubes in the inner of copolymer with diameters ranging between 90 and 100 nm were observed. The overall morphology of the previously synthetized nanotubes was determined by scanning electron microscopy (SEM). For the nanocomposite system, the morphology was studied by atomic force microscopy (AFM) from which a grain shape structure was observed. This process resulted in a new nanocompsite material with an average grain diameter estimated by SEM and AFM ranging between 210-240 nm. It was observed that the nanotubes were homogeneously dispersed within the polymeric matrix. The prepared material could be suitable in the design of electronic devices and additionally could have potential applications as biomaterial.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.62 n.3 20172017-09-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072017000303634en10.4067/s0717-97072017000303634
institution	Scielo Chile
collection	Scielo Chile
language	English
topic	polymer nanocomposite morphological characterization TiO2 nanotubes
spellingShingle	polymer nanocomposite morphological characterization TiO2 nanotubes OYARZÚN,DIEGO P. PIZARRO,GUADALUPE DEL C. ASENJO,ANDRÉS TELLO,ALEJANDRA MARTIN-TRASANCO,RUDY ZÚÑIGA,CÉSAR SÁNCHEZ,JULIO ARRATIA-PEREZ,RAMIRO SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)
description	ABSTRACT In this study, we examined the synthesis, and characterization of TiO2/poly(N-maleoylglycine-co-acrylic acid) (TiO2/poly(MG-co-AA)) nanocomposite. The nanocomposite was prepared by the dispersion of TiO2 nanotubes in a water solution of the polymer (3% w/w) and then it was lyophilized. The nanocomposite was characterized by FTIR and Raman spectroscopies. The incorporation of TiO2 nanotubes to the polymeric matrix was determined by transmission electron microscopy (TEM) from which TiO2 nanotubes in the inner of copolymer with diameters ranging between 90 and 100 nm were observed. The overall morphology of the previously synthetized nanotubes was determined by scanning electron microscopy (SEM). For the nanocomposite system, the morphology was studied by atomic force microscopy (AFM) from which a grain shape structure was observed. This process resulted in a new nanocompsite material with an average grain diameter estimated by SEM and AFM ranging between 210-240 nm. It was observed that the nanotubes were homogeneously dispersed within the polymeric matrix. The prepared material could be suitable in the design of electronic devices and additionally could have potential applications as biomaterial.
author	OYARZÚN,DIEGO P. PIZARRO,GUADALUPE DEL C. ASENJO,ANDRÉS TELLO,ALEJANDRA MARTIN-TRASANCO,RUDY ZÚÑIGA,CÉSAR SÁNCHEZ,JULIO ARRATIA-PEREZ,RAMIRO
author_facet	OYARZÚN,DIEGO P. PIZARRO,GUADALUPE DEL C. ASENJO,ANDRÉS TELLO,ALEJANDRA MARTIN-TRASANCO,RUDY ZÚÑIGA,CÉSAR SÁNCHEZ,JULIO ARRATIA-PEREZ,RAMIRO
author_sort	OYARZÚN,DIEGO P.
title	SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)
title_short	SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)
title_full	SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)
title_fullStr	SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)
title_full_unstemmed	SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)
title_sort	synthesis and morphological characterization of nanocomposite based on anodic tio2 nanotubes and poly(n-maleoyl glycine-co-acrylic acid)
publisher	Sociedad Chilena de Química
publishDate	2017
url	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072017000303634
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SYNTHESIS AND MORPHOLOGICAL CHARACTERIZATION OF NANOCOMPOSITE BASED ON ANODIC TiO2 NANOTUBES AND POLY(N-MALEOYL GLYCINE-CO-ACRYLIC ACID)

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