NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE

ABSTRACT Single crystals of 1,3-bis(cyanomethoxy)calix[4]arene (1) were grown from Chloroform/Methanol mixture and these were nanodecorated with colloidal gold nanoparticles (AuNps). The single crystals were then characterized by single-crystal X-ray diffraction (XRD) and Scanning Electronic Microsc...

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Autores principales:	MORIS,S., SILVA,N., SAITZ,C., JARA,P., CHORNIK,B.
Lenguaje:	English
Publicado:	Sociedad Chilena de Química 2017
Materias:	Single crystals 1,3-bis(cyanomeththoxy)calix[4]arene nanodecorated Gold Nanoparticles
Acceso en línea:	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072017000403772
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spelling	oai:scielo:S0717-970720170004037722018-04-02NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENEMORIS,S.SILVA,N.SAITZ,C.JARA,P.CHORNIK,B. Single crystals 1,3-bis(cyanomeththoxy)calix[4]arene nanodecorated Gold Nanoparticles ABSTRACT Single crystals of 1,3-bis(cyanomethoxy)calix[4]arene (1) were grown from Chloroform/Methanol mixture and these were nanodecorated with colloidal gold nanoparticles (AuNps). The single crystals were then characterized by single-crystal X-ray diffraction (XRD) and Scanning Electronic Microscopy (SEM). The nanodecorated crystals were characterized by UV-Visible Absorption Spectroscopy, Transmission Electronic Microscopy (TEM) and X-ray Photoelectron Spectroscopy (XPS). In this work, it is shown that the stabilization of the nanoparticles occurs through of the interactions of these with the nitrile group, maintaining their shape and size.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.62 n.4 20172017-12-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072017000403772en10.4067/s0717-97072017000403772
institution	Scielo Chile
collection	Scielo Chile
language	English
topic	Single crystals 1,3-bis(cyanomeththoxy)calix[4]arene nanodecorated Gold Nanoparticles
spellingShingle	Single crystals 1,3-bis(cyanomeththoxy)calix[4]arene nanodecorated Gold Nanoparticles MORIS,S. SILVA,N. SAITZ,C. JARA,P. CHORNIK,B. NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE
description	ABSTRACT Single crystals of 1,3-bis(cyanomethoxy)calix[4]arene (1) were grown from Chloroform/Methanol mixture and these were nanodecorated with colloidal gold nanoparticles (AuNps). The single crystals were then characterized by single-crystal X-ray diffraction (XRD) and Scanning Electronic Microscopy (SEM). The nanodecorated crystals were characterized by UV-Visible Absorption Spectroscopy, Transmission Electronic Microscopy (TEM) and X-ray Photoelectron Spectroscopy (XPS). In this work, it is shown that the stabilization of the nanoparticles occurs through of the interactions of these with the nitrile group, maintaining their shape and size.
author	MORIS,S. SILVA,N. SAITZ,C. JARA,P. CHORNIK,B.
author_facet	MORIS,S. SILVA,N. SAITZ,C. JARA,P. CHORNIK,B.
author_sort	MORIS,S.
title	NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE
title_short	NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE
title_full	NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE
title_fullStr	NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE
title_full_unstemmed	NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE
title_sort	nanodecoration of single crystals of 5,11,17,23-tetra-tert-butyl-25,27-bis(cyanomethoxy)-26, 28-dihydroxycalix[4]arene
publisher	Sociedad Chilena de Química
publishDate	2017
url	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072017000403772
work_keys_str_mv	AT moriss nanodecorationofsinglecrystalsof5111723tetratertbutyl2527biscyanomethoxy2628dihydroxycalix4arene AT silvan nanodecorationofsinglecrystalsof5111723tetratertbutyl2527biscyanomethoxy2628dihydroxycalix4arene AT saitzc nanodecorationofsinglecrystalsof5111723tetratertbutyl2527biscyanomethoxy2628dihydroxycalix4arene AT jarap nanodecorationofsinglecrystalsof5111723tetratertbutyl2527biscyanomethoxy2628dihydroxycalix4arene AT chornikb nanodecorationofsinglecrystalsof5111723tetratertbutyl2527biscyanomethoxy2628dihydroxycalix4arene
_version_	1714200919859527680

NANODECORATION OF SINGLE CRYSTALS OF 5,11,17,23-TETRA-TERT-BUTYL-25,27-BIS(CYANOMETHOXY)-26, 28-DIHYDROXYCALIX[4]ARENE

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