INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVES
ABSTRACT In this study, an effective method for the synthesis of pyranopyrimidinone and xanthene derivatives is introduced. In this method, zinc oxide-chitosan nanocomposite has been used as a catalyst and all reactions were performed under irradiated in a microwave oven at a power of 230W. The prop...
Guardado en:
Autores principales: | , , |
---|---|
Lenguaje: | English |
Publicado: |
Sociedad Chilena de Química
2019
|
Materias: | |
Acceso en línea: | http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072019000404633 |
Etiquetas: |
Agregar Etiqueta
Sin Etiquetas, Sea el primero en etiquetar este registro!
|
id |
oai:scielo:S0717-97072019000404633 |
---|---|
record_format |
dspace |
spelling |
oai:scielo:S0717-970720190004046332020-02-03INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVESAmininia,A.Pourshamsian,K.Sadeghi,B. Zinc oxide-chitosan nanocomposite microwave pyranopyrimidinone xanthene Biological activity MIC MBC ABSTRACT In this study, an effective method for the synthesis of pyranopyrimidinone and xanthene derivatives is introduced. In this method, zinc oxide-chitosan nanocomposite has been used as a catalyst and all reactions were performed under irradiated in a microwave oven at a power of 230W. The properties of zinc oxide-chitosan nanocomposite were characterized by X-ray diffraction (XRD), energy dispersive X-ray (EDAX) analysis and scanning electron microscopy (SEM). The results indicated that the size of zinc oxide-chitosan nanocomposite varies between 76–95 nm. The catalyst activity has maintained its activity after four runs. The main advantages of this method are; Eco-friendly procedure, catalytic synthesis of affordable and inexpensive materials, short reaction time, and excellent yields which makes it more economic than the other conventional methods. The antibacterial activity of the products was investigated using Minimum Inhibitory Concentration (MIC) and the Minimum Bactericidal Concentration (MBC) methods. Pyranopyrimidinone derivatives exhibit more antibacterial activity.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.64 n.4 20192019-12-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072019000404633en10.4067/S0717-97072019000404633 |
institution |
Scielo Chile |
collection |
Scielo Chile |
language |
English |
topic |
Zinc oxide-chitosan nanocomposite microwave pyranopyrimidinone xanthene Biological activity MIC MBC |
spellingShingle |
Zinc oxide-chitosan nanocomposite microwave pyranopyrimidinone xanthene Biological activity MIC MBC Amininia,A. Pourshamsian,K. Sadeghi,B. INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVES |
description |
ABSTRACT In this study, an effective method for the synthesis of pyranopyrimidinone and xanthene derivatives is introduced. In this method, zinc oxide-chitosan nanocomposite has been used as a catalyst and all reactions were performed under irradiated in a microwave oven at a power of 230W. The properties of zinc oxide-chitosan nanocomposite were characterized by X-ray diffraction (XRD), energy dispersive X-ray (EDAX) analysis and scanning electron microscopy (SEM). The results indicated that the size of zinc oxide-chitosan nanocomposite varies between 76–95 nm. The catalyst activity has maintained its activity after four runs. The main advantages of this method are; Eco-friendly procedure, catalytic synthesis of affordable and inexpensive materials, short reaction time, and excellent yields which makes it more economic than the other conventional methods. The antibacterial activity of the products was investigated using Minimum Inhibitory Concentration (MIC) and the Minimum Bactericidal Concentration (MBC) methods. Pyranopyrimidinone derivatives exhibit more antibacterial activity. |
author |
Amininia,A. Pourshamsian,K. Sadeghi,B. |
author_facet |
Amininia,A. Pourshamsian,K. Sadeghi,B. |
author_sort |
Amininia,A. |
title |
INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVES |
title_short |
INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVES |
title_full |
INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVES |
title_fullStr |
INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVES |
title_full_unstemmed |
INTRODUCING AN EFFECTIVE NANOCATALYTIC FOR THE ONE-POT SYNTHESIS AND INVESTIGATION OF BIOLOGICAL PROPERTIES OF PYRANOPYRIMIDINONE AND XANTHENE DERIVATIVES |
title_sort |
introducing an effective nanocatalytic for the one-pot synthesis and investigation of biological properties of pyranopyrimidinone and xanthene derivatives |
publisher |
Sociedad Chilena de Química |
publishDate |
2019 |
url |
http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072019000404633 |
work_keys_str_mv |
AT amininiaa introducinganeffectivenanocatalyticfortheonepotsynthesisandinvestigationofbiologicalpropertiesofpyranopyrimidinoneandxanthenederivatives AT pourshamsiank introducinganeffectivenanocatalyticfortheonepotsynthesisandinvestigationofbiologicalpropertiesofpyranopyrimidinoneandxanthenederivatives AT sadeghib introducinganeffectivenanocatalyticfortheonepotsynthesisandinvestigationofbiologicalpropertiesofpyranopyrimidinoneandxanthenederivatives |
_version_ |
1714200943579365376 |