Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistance

ABSTRACT This article aimed to analyze the effect of the thermal oxidation in the corrosion resistance and the hardness properties of TiO2 nanostructures obtained by the anodizing process in the HF/H3PO4 solution TiO2 nanostructures on Ti6Al4V obtained by anodizing processes were subjected to therma...

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Autores principales: Muñoz-Mizuno,Andrea, Cely-Bautista,Mercedes, Jaramillo-Colpas,Javier, Hincapie,Duberney, Calderón-Hernández,José Wilmar
Lenguaje:English
Publicado: Universidad de Tarapacá. 2020
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EIS
Acceso en línea:http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0718-33052020000300362
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spelling oai:scielo:S0718-330520200003003622020-11-03Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistanceMuñoz-Mizuno,AndreaCely-Bautista,MercedesJaramillo-Colpas,JavierHincapie,DuberneyCalderón-Hernández,José Wilmar Nanostructures TiO2 nanohardness EIS thermal oxidation ABSTRACT This article aimed to analyze the effect of the thermal oxidation in the corrosion resistance and the hardness properties of TiO2 nanostructures obtained by the anodizing process in the HF/H3PO4 solution TiO2 nanostructures on Ti6Al4V obtained by anodizing processes were subjected to thermal oxidation (TO) treatments over a temperature range from 500 °C to 620 °C for 2 hours. Surface morphology was evaluated by using scanning electron microscopy; the hardness properties of TiO2 nanostructures were obtained by Nanoindentation measurements using a Berkovich probe with a tip radius of 150 mm. The corrosion behavior of the samples was studied using potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). The results showed that TiO2 nanostructures, modified by thermal oxidation, increased the surface properties of hardness and corrosion resistance, compared to the substrate, maintaining its mixed or tubular structure. On the other hand, a transformation of nanotubes to nanopores after 600°C was evidenced, generating significant changes in the mechanical properties of these structures.info:eu-repo/semantics/openAccessUniversidad de Tarapacá.Ingeniare. Revista chilena de ingeniería v.28 n.3 20202020-09-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0718-33052020000300362en10.4067/S0718-33052020000300362
institution Scielo Chile
collection Scielo Chile
language English
topic Nanostructures
TiO2
nanohardness
EIS
thermal oxidation
spellingShingle Nanostructures
TiO2
nanohardness
EIS
thermal oxidation
Muñoz-Mizuno,Andrea
Cely-Bautista,Mercedes
Jaramillo-Colpas,Javier
Hincapie,Duberney
Calderón-Hernández,José Wilmar
Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistance
description ABSTRACT This article aimed to analyze the effect of the thermal oxidation in the corrosion resistance and the hardness properties of TiO2 nanostructures obtained by the anodizing process in the HF/H3PO4 solution TiO2 nanostructures on Ti6Al4V obtained by anodizing processes were subjected to thermal oxidation (TO) treatments over a temperature range from 500 °C to 620 °C for 2 hours. Surface morphology was evaluated by using scanning electron microscopy; the hardness properties of TiO2 nanostructures were obtained by Nanoindentation measurements using a Berkovich probe with a tip radius of 150 mm. The corrosion behavior of the samples was studied using potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). The results showed that TiO2 nanostructures, modified by thermal oxidation, increased the surface properties of hardness and corrosion resistance, compared to the substrate, maintaining its mixed or tubular structure. On the other hand, a transformation of nanotubes to nanopores after 600°C was evidenced, generating significant changes in the mechanical properties of these structures.
author Muñoz-Mizuno,Andrea
Cely-Bautista,Mercedes
Jaramillo-Colpas,Javier
Hincapie,Duberney
Calderón-Hernández,José Wilmar
author_facet Muñoz-Mizuno,Andrea
Cely-Bautista,Mercedes
Jaramillo-Colpas,Javier
Hincapie,Duberney
Calderón-Hernández,José Wilmar
author_sort Muñoz-Mizuno,Andrea
title Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistance
title_short Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistance
title_full Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistance
title_fullStr Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistance
title_full_unstemmed Effect on thermal oxidation in TiO2 nanostructures on nanohardness and corrosion resistance
title_sort effect on thermal oxidation in tio2 nanostructures on nanohardness and corrosion resistance
publisher Universidad de Tarapacá.
publishDate 2020
url http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0718-33052020000300362
work_keys_str_mv AT munozmizunoandrea effectonthermaloxidationintio2nanostructuresonnanohardnessandcorrosionresistance
AT celybautistamercedes effectonthermaloxidationintio2nanostructuresonnanohardnessandcorrosionresistance
AT jaramillocolpasjavier effectonthermaloxidationintio2nanostructuresonnanohardnessandcorrosionresistance
AT hincapieduberney effectonthermaloxidationintio2nanostructuresonnanohardnessandcorrosionresistance
AT calderonhernandezjosewilmar effectonthermaloxidationintio2nanostructuresonnanohardnessandcorrosionresistance
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