LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)

A simultaneous analysis method using LC-MS/MS and GC-MS/MS was developed for improving the analysis accuracy of various pesticide residues. Samples spiked with 247 and 34 pesticide residues were analyzed by LC-MS/MS and GC-MS/MS, respectively. The method was verified by measuring sensitivity, linear...

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Autores principales:	Ji Eun Lee, Sung Ho Jang, Suel Hye Hur, Han Yeol Bang, In-kyung Bae, Ho Jin Kim
Formato:	article
Lenguaje:	EN
Publicado:	Taylor & Francis Group 2021
Materias:	gc-ms/ms lc-ms/ms cross-checking pesticide sweet peppe Nutrition. Foods and food supply TX341-641 Food processing and manufacture TP368-456
Acceso en línea:	https://doaj.org/article/0dc0f9c35dcb4e4ab9a9c84ff8a093fd
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spelling	oai:doaj.org-article:0dc0f9c35dcb4e4ab9a9c84ff8a093fd2021-11-26T11:19:47ZLC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)1094-29121532-238610.1080/10942912.2021.1993251https://doaj.org/article/0dc0f9c35dcb4e4ab9a9c84ff8a093fd2021-01-01T00:00:00Zhttp://dx.doi.org/10.1080/10942912.2021.1993251https://doaj.org/toc/1094-2912https://doaj.org/toc/1532-2386A simultaneous analysis method using LC-MS/MS and GC-MS/MS was developed for improving the analysis accuracy of various pesticide residues. Samples spiked with 247 and 34 pesticide residues were analyzed by LC-MS/MS and GC-MS/MS, respectively. The method was verified by measuring sensitivity, linearity, selectivity, precision, and accuracy. LC-MS/MS LOD and LOQ values were determined to be 0.03–0.5 μg/kg, and 0.6–1.5 μg/kg, respectively, while the corresponding values for GC-MS/MS were found to be 0.9–2.0 μg/kg and from 3.0–5.7 μg/kg, respectively. Most of the 34 common residues had recovery rates of 70–120%. The results showed that the developed method can be a reliable and more accurate than the general multi component analysis method.Ji Eun LeeSung Ho JangSuel Hye HurHan Yeol BangIn-kyung BaeHo Jin KimTaylor & Francis Grouparticlegc-ms/mslc-ms/mscross-checkingpesticidesweet peppeNutrition. Foods and food supplyTX341-641Food processing and manufactureTP368-456ENInternational Journal of Food Properties, Vol 24, Iss 1, Pp 1758-1776 (2021)
institution	DOAJ
collection	DOAJ
language	EN
topic	gc-ms/ms lc-ms/ms cross-checking pesticide sweet peppe Nutrition. Foods and food supply TX341-641 Food processing and manufacture TP368-456
spellingShingle	gc-ms/ms lc-ms/ms cross-checking pesticide sweet peppe Nutrition. Foods and food supply TX341-641 Food processing and manufacture TP368-456 Ji Eun Lee Sung Ho Jang Suel Hye Hur Han Yeol Bang In-kyung Bae Ho Jin Kim LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)
description	A simultaneous analysis method using LC-MS/MS and GC-MS/MS was developed for improving the analysis accuracy of various pesticide residues. Samples spiked with 247 and 34 pesticide residues were analyzed by LC-MS/MS and GC-MS/MS, respectively. The method was verified by measuring sensitivity, linearity, selectivity, precision, and accuracy. LC-MS/MS LOD and LOQ values were determined to be 0.03–0.5 μg/kg, and 0.6–1.5 μg/kg, respectively, while the corresponding values for GC-MS/MS were found to be 0.9–2.0 μg/kg and from 3.0–5.7 μg/kg, respectively. Most of the 34 common residues had recovery rates of 70–120%. The results showed that the developed method can be a reliable and more accurate than the general multi component analysis method.
format	article
author	Ji Eun Lee Sung Ho Jang Suel Hye Hur Han Yeol Bang In-kyung Bae Ho Jin Kim
author_facet	Ji Eun Lee Sung Ho Jang Suel Hye Hur Han Yeol Bang In-kyung Bae Ho Jin Kim
author_sort	Ji Eun Lee
title	LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)
title_short	LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)
title_full	LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)
title_fullStr	LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)
title_full_unstemmed	LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)
title_sort	lc-ms/ms and gc-ms/ms cross-checking analysis method for 247 pesticide residues in sweet pepper (capsicum annuum)
publisher	Taylor & Francis Group
publishDate	2021
url	https://doaj.org/article/0dc0f9c35dcb4e4ab9a9c84ff8a093fd
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LC-MS/MS and GC-MS/MS cross-checking analysis method for 247 pesticide residues in sweet pepper (Capsicum annuum)

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