POLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS

The presence of polycyclic aromatic hydrocarbons (PAHs) and heavy metals in smoked food in appreciable amount is an issue of concern in recent times. The present study focuses on the PAHs and heavy metal contents of smoked beef. The effect of three solvent combinations (n-hexane, dichloromethane and...

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Autores principales: Abel INOBEME, Alexander Ikechukwu AJAI, Abdullahi MANN, Yahaya Ahmed IYAKA
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Lenguaje:EN
Publicado: Stefan cel Mare University of Suceava 2019
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Acceso en línea:https://doaj.org/article/31843e1a94f148c2949d25d43ec255a2
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spelling oai:doaj.org-article:31843e1a94f148c2949d25d43ec255a22021-12-02T19:27:32ZPOLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS2068-66092559-6381https://doaj.org/article/31843e1a94f148c2949d25d43ec255a22019-06-01T00:00:00Zhttp://www.fia.usv.ro/fiajournal/index.php/FENS/article/view/644/598https://doaj.org/toc/2068-6609https://doaj.org/toc/2559-6381The presence of polycyclic aromatic hydrocarbons (PAHs) and heavy metals in smoked food in appreciable amount is an issue of concern in recent times. The present study focuses on the PAHs and heavy metal contents of smoked beef. The effect of three solvent combinations (n-hexane, dichloromethane and n-hexane:DCM) and two extraction methods (Soxhlet and sonication) on PAHs contents were also assessed. GC-MS was used for the quantification of PAHs while heavy metal contents were analyzed using atomic absorption spectrometer. The concentrations of metals were in the general order: Fe > Zn> Mn >Pb > Cu > Cd. The content of metals was generally lower than the permissible limits based on international standard. Sonication method gave the highest yield of total PAHs (45.15µg/kg) while n-hexane registered the highest extraction efficiency amongst solvents. The concentration of PAHs ranged between 0.09 - 9.90 µg/kg. Benzo[a] pyrene exceeded the 5.0µg/kg maximum limit in some cases. It is necessary to continually check the concentrations of PAHs and heavy metals in food.Abel INOBEMEAlexander Ikechukwu AJAIAbdullahi MANNYahaya Ahmed IYAKAStefan cel Mare University of Suceavaarticlesmokingextractionheavy metalsbeefpolycyclic aromatic hydrocarbonsFood processing and manufactureTP368-456ENFood and Environment Safety, Vol 18, Iss 2, Pp 111-122 (2019)
institution DOAJ
collection DOAJ
language EN
topic smoking
extraction
heavy metals
beef
polycyclic aromatic hydrocarbons
Food processing and manufacture
TP368-456
spellingShingle smoking
extraction
heavy metals
beef
polycyclic aromatic hydrocarbons
Food processing and manufacture
TP368-456
Abel INOBEME
Alexander Ikechukwu AJAI
Abdullahi MANN
Yahaya Ahmed IYAKA
POLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS
description The presence of polycyclic aromatic hydrocarbons (PAHs) and heavy metals in smoked food in appreciable amount is an issue of concern in recent times. The present study focuses on the PAHs and heavy metal contents of smoked beef. The effect of three solvent combinations (n-hexane, dichloromethane and n-hexane:DCM) and two extraction methods (Soxhlet and sonication) on PAHs contents were also assessed. GC-MS was used for the quantification of PAHs while heavy metal contents were analyzed using atomic absorption spectrometer. The concentrations of metals were in the general order: Fe > Zn> Mn >Pb > Cu > Cd. The content of metals was generally lower than the permissible limits based on international standard. Sonication method gave the highest yield of total PAHs (45.15µg/kg) while n-hexane registered the highest extraction efficiency amongst solvents. The concentration of PAHs ranged between 0.09 - 9.90 µg/kg. Benzo[a] pyrene exceeded the 5.0µg/kg maximum limit in some cases. It is necessary to continually check the concentrations of PAHs and heavy metals in food.
format article
author Abel INOBEME
Alexander Ikechukwu AJAI
Abdullahi MANN
Yahaya Ahmed IYAKA
author_facet Abel INOBEME
Alexander Ikechukwu AJAI
Abdullahi MANN
Yahaya Ahmed IYAKA
author_sort Abel INOBEME
title POLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS
title_short POLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS
title_full POLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS
title_fullStr POLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS
title_full_unstemmed POLYCYCLIC AROMATIC HYDROCARBONS AND HEAVY METALS IN SMOKED BEEF: EFFECT OF SOLVENTS AND EXTRACTION METHODS
title_sort polycyclic aromatic hydrocarbons and heavy metals in smoked beef: effect of solvents and extraction methods
publisher Stefan cel Mare University of Suceava
publishDate 2019
url https://doaj.org/article/31843e1a94f148c2949d25d43ec255a2
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AT abdullahimann polycyclicaromatichydrocarbonsandheavymetalsinsmokedbeefeffectofsolventsandextractionmethods
AT yahayaahmediyaka polycyclicaromatichydrocarbonsandheavymetalsinsmokedbeefeffectofsolventsandextractionmethods
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