VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES
A high performance liquid chromatography method for carbendazim residues determination was adapted to the condition of our laboratory and validated for tomatoes samples. Carbendazim eluted at 3.13 minutes. The signal was linear over the concentration range 1 to 15 µg/ml with correlation coefficient...
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Stefan cel Mare University of Suceava
2018
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oai:doaj.org-article:6fc8695575d545b1826e98694542de052021-12-02T19:35:52ZVALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES2068-66092559-6381https://doaj.org/article/6fc8695575d545b1826e98694542de052018-09-01T00:00:00Zhttp://www.fia.usv.ro/fiajournal/index.php/FENS/article/view/601https://doaj.org/toc/2068-6609https://doaj.org/toc/2559-6381A high performance liquid chromatography method for carbendazim residues determination was adapted to the condition of our laboratory and validated for tomatoes samples. Carbendazim eluted at 3.13 minutes. The signal was linear over the concentration range 1 to 15 µg/ml with correlation coefficient 0.999092. The detection limit and the quantitation limit values were 0.002 mg/kg and 0.02 mg/kg respectively. Relative standard deviation of repeatability was 3.47% and 4.78% and recovery was 99.67% and 113,11% for two levels of concentration. The adapted method allowed a simple and rapid separation and quantification of carbendazim in tomatoes by high performance liquid chromatography.Veronica TANASAMadalina DOLTUDorin SORARadu I. TANASANarcisa BABEANUStefan cel Mare University of Suceavaarticlecarbendazimtomatoesvalidation parametersHPLCFood processing and manufactureTP368-456ENFood and Environment Safety, Vol 17, Iss 3, Pp 327- 331 (2018) |
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carbendazim tomatoes validation parameters HPLC Food processing and manufacture TP368-456 |
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carbendazim tomatoes validation parameters HPLC Food processing and manufacture TP368-456 Veronica TANASA Madalina DOLTU Dorin SORA Radu I. TANASA Narcisa BABEANU VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES |
description |
A high performance liquid chromatography method for carbendazim residues determination was adapted to the condition of our laboratory and validated for tomatoes samples. Carbendazim eluted at 3.13 minutes. The signal was linear over the concentration range 1 to 15 µg/ml with correlation coefficient 0.999092. The detection limit and the quantitation limit values were 0.002 mg/kg and 0.02 mg/kg respectively. Relative standard deviation of repeatability was 3.47% and 4.78% and recovery was 99.67% and 113,11% for two levels of concentration. The adapted method allowed a simple and rapid separation and quantification of carbendazim in tomatoes by high performance liquid chromatography. |
format |
article |
author |
Veronica TANASA Madalina DOLTU Dorin SORA Radu I. TANASA Narcisa BABEANU |
author_facet |
Veronica TANASA Madalina DOLTU Dorin SORA Radu I. TANASA Narcisa BABEANU |
author_sort |
Veronica TANASA |
title |
VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES |
title_short |
VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES |
title_full |
VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES |
title_fullStr |
VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES |
title_full_unstemmed |
VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES |
title_sort |
validation of a high performance liquid chromatography method for carbendazim residues quantification in tomatoes |
publisher |
Stefan cel Mare University of Suceava |
publishDate |
2018 |
url |
https://doaj.org/article/6fc8695575d545b1826e98694542de05 |
work_keys_str_mv |
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1718376387125968896 |