VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES

A high performance liquid chromatography method for carbendazim residues determination was adapted to the condition of our laboratory and validated for tomatoes samples. Carbendazim eluted at 3.13 minutes. The signal was linear over the concentration range 1 to 15 µg/ml with correlation coefficient...

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Autores principales: Veronica TANASA, Madalina DOLTU, Dorin SORA, Radu I. TANASA, Narcisa BABEANU
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Lenguaje:EN
Publicado: Stefan cel Mare University of Suceava 2018
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Acceso en línea:https://doaj.org/article/6fc8695575d545b1826e98694542de05
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spelling oai:doaj.org-article:6fc8695575d545b1826e98694542de052021-12-02T19:35:52ZVALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES2068-66092559-6381https://doaj.org/article/6fc8695575d545b1826e98694542de052018-09-01T00:00:00Zhttp://www.fia.usv.ro/fiajournal/index.php/FENS/article/view/601https://doaj.org/toc/2068-6609https://doaj.org/toc/2559-6381A high performance liquid chromatography method for carbendazim residues determination was adapted to the condition of our laboratory and validated for tomatoes samples. Carbendazim eluted at 3.13 minutes. The signal was linear over the concentration range 1 to 15 µg/ml with correlation coefficient 0.999092. The detection limit and the quantitation limit values were 0.002 mg/kg and 0.02 mg/kg respectively. Relative standard deviation of repeatability was 3.47% and 4.78% and recovery was 99.67% and 113,11% for two levels of concentration. The adapted method allowed a simple and rapid separation and quantification of carbendazim in tomatoes by high performance liquid chromatography.Veronica TANASAMadalina DOLTUDorin SORARadu I. TANASANarcisa BABEANUStefan cel Mare University of Suceavaarticlecarbendazimtomatoesvalidation parametersHPLCFood processing and manufactureTP368-456ENFood and Environment Safety, Vol 17, Iss 3, Pp 327- 331 (2018)
institution DOAJ
collection DOAJ
language EN
topic carbendazim
tomatoes
validation parameters
HPLC
Food processing and manufacture
TP368-456
spellingShingle carbendazim
tomatoes
validation parameters
HPLC
Food processing and manufacture
TP368-456
Veronica TANASA
Madalina DOLTU
Dorin SORA
Radu I. TANASA
Narcisa BABEANU
VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES
description A high performance liquid chromatography method for carbendazim residues determination was adapted to the condition of our laboratory and validated for tomatoes samples. Carbendazim eluted at 3.13 minutes. The signal was linear over the concentration range 1 to 15 µg/ml with correlation coefficient 0.999092. The detection limit and the quantitation limit values were 0.002 mg/kg and 0.02 mg/kg respectively. Relative standard deviation of repeatability was 3.47% and 4.78% and recovery was 99.67% and 113,11% for two levels of concentration. The adapted method allowed a simple and rapid separation and quantification of carbendazim in tomatoes by high performance liquid chromatography.
format article
author Veronica TANASA
Madalina DOLTU
Dorin SORA
Radu I. TANASA
Narcisa BABEANU
author_facet Veronica TANASA
Madalina DOLTU
Dorin SORA
Radu I. TANASA
Narcisa BABEANU
author_sort Veronica TANASA
title VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES
title_short VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES
title_full VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES
title_fullStr VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES
title_full_unstemmed VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES
title_sort validation of a high performance liquid chromatography method for carbendazim residues quantification in tomatoes
publisher Stefan cel Mare University of Suceava
publishDate 2018
url https://doaj.org/article/6fc8695575d545b1826e98694542de05
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