Characteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)

Abstract. Rahayu PP, Rosyidi D, Purwadi, Thohari I. 2019. Characteristics of catechin extracted from cocoa husks using microwave-assisted extraction (MAE). Biodiversitas 20: 3626-3631. Cocoa husks, a by-product of cocoa processing, were investigated as a source of catechin. The objective of this res...

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Autores principales: djalal rosyidi, DJALAL ROSYIDI, PURWADI, IMAM THOHARI
Formato: article
Lenguaje:EN
Publicado: MBI & UNS Solo 2019
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Acceso en línea:https://doaj.org/article/797983e306f846ebaa4944c830d40626
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spelling oai:doaj.org-article:797983e306f846ebaa4944c830d406262021-11-21T21:59:05ZCharacteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)1412-033X2085-472210.13057/biodiv/d201222https://doaj.org/article/797983e306f846ebaa4944c830d406262019-11-01T00:00:00Zhttps://smujo.id/biodiv/article/view/4504https://doaj.org/toc/1412-033Xhttps://doaj.org/toc/2085-4722Abstract. Rahayu PP, Rosyidi D, Purwadi, Thohari I. 2019. Characteristics of catechin extracted from cocoa husks using microwave-assisted extraction (MAE). Biodiversitas 20: 3626-3631. Cocoa husks, a by-product of cocoa processing, were investigated as a source of catechin. The objective of this research was to investigate the best extraction time for catechin of cocoa husk using microwave-assisted extraction (MAE). Four different treatments (4, 6, 8, and 10 min) were tested. Catechin was analyzed using Fourier transform infrared (FTIR) spectroscopy, and total phenol content (TPC) and total catechin content (TCC) were determined by liquid chromatography-mass spectrometry (LC-MS). The longest extraction time (10 min) produced the highest phenolic content, although it was similar to that obtained at 8 min. The IR spectra of the cocoa husk extract were stable for the 4, 6, and 8 min extractions. However, the spectra after the 10 min extraction showed more peaks, especially for phenolic compounds and catechins. The mass spectra of catechin showed a peak at RT 3.11 and a protonated ion peak [M+H]+ at m/z 307. The results for TPC, TCC, FTIR, and LC-MS indicated that a 10 min extraction using MAE was the optimum treatment.djalal rosyidiDJALAL ROSYIDIPURWADIIMAM THOHARIMBI & UNS Soloarticlecatechin, cocoa husk extract, extraction time, ir spectra, polyphenolBiology (General)QH301-705.5ENBiodiversitas, Vol 20, Iss 12 (2019)
institution DOAJ
collection DOAJ
language EN
topic catechin, cocoa husk extract, extraction time, ir spectra, polyphenol
Biology (General)
QH301-705.5
spellingShingle catechin, cocoa husk extract, extraction time, ir spectra, polyphenol
Biology (General)
QH301-705.5
djalal rosyidi
DJALAL ROSYIDI
PURWADI
IMAM THOHARI
Characteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)
description Abstract. Rahayu PP, Rosyidi D, Purwadi, Thohari I. 2019. Characteristics of catechin extracted from cocoa husks using microwave-assisted extraction (MAE). Biodiversitas 20: 3626-3631. Cocoa husks, a by-product of cocoa processing, were investigated as a source of catechin. The objective of this research was to investigate the best extraction time for catechin of cocoa husk using microwave-assisted extraction (MAE). Four different treatments (4, 6, 8, and 10 min) were tested. Catechin was analyzed using Fourier transform infrared (FTIR) spectroscopy, and total phenol content (TPC) and total catechin content (TCC) were determined by liquid chromatography-mass spectrometry (LC-MS). The longest extraction time (10 min) produced the highest phenolic content, although it was similar to that obtained at 8 min. The IR spectra of the cocoa husk extract were stable for the 4, 6, and 8 min extractions. However, the spectra after the 10 min extraction showed more peaks, especially for phenolic compounds and catechins. The mass spectra of catechin showed a peak at RT 3.11 and a protonated ion peak [M+H]+ at m/z 307. The results for TPC, TCC, FTIR, and LC-MS indicated that a 10 min extraction using MAE was the optimum treatment.
format article
author djalal rosyidi
DJALAL ROSYIDI
PURWADI
IMAM THOHARI
author_facet djalal rosyidi
DJALAL ROSYIDI
PURWADI
IMAM THOHARI
author_sort djalal rosyidi
title Characteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)
title_short Characteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)
title_full Characteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)
title_fullStr Characteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)
title_full_unstemmed Characteristics of catechin extracted from cocoa husks using microwave assisted extraction (MAE)
title_sort characteristics of catechin extracted from cocoa husks using microwave assisted extraction (mae)
publisher MBI & UNS Solo
publishDate 2019
url https://doaj.org/article/797983e306f846ebaa4944c830d40626
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AT djalalrosyidi characteristicsofcatechinextractedfromcocoahusksusingmicrowaveassistedextractionmae
AT purwadi characteristicsofcatechinextractedfromcocoahusksusingmicrowaveassistedextractionmae
AT imamthohari characteristicsofcatechinextractedfromcocoahusksusingmicrowaveassistedextractionmae
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