Recovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity

Phenolic compounds recovery by mechanical stirring extraction (MSE) was studied from orange and spinach wastes using water as a solvent. The statistical analysis showed that the highest total polyphenol content (TPC) yield was obtained using 15 min, 70 °C, 1:100 (<i>w/v</i>) solid/solven...

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Autores principales: María Fernanda Montenegro-Landívar, Paulina Tapia-Quirós, Xanel Vecino, Mònica Reig, César Valderrama, Mercè Granados, José Luis Cortina, Javier Saurina
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Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:7d523a7c4f1c4bb2833acf3b25d46ec62021-11-25T16:28:47ZRecovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity10.3390/antiox101118002076-3921https://doaj.org/article/7d523a7c4f1c4bb2833acf3b25d46ec62021-11-01T00:00:00Zhttps://www.mdpi.com/2076-3921/10/11/1800https://doaj.org/toc/2076-3921Phenolic compounds recovery by mechanical stirring extraction (MSE) was studied from orange and spinach wastes using water as a solvent. The statistical analysis showed that the highest total polyphenol content (TPC) yield was obtained using 15 min, 70 °C, 1:100 (<i>w/v</i>) solid/solvent ratio and pH 4 for orange; and 5 min, 50 °C, 1:50 (<i>w/v</i>) solid/solvent ratio and pH 6 for spinach. Under these conditions, the TPC was 1 mg gallic acid equivalent (GAE) g<sup>−1</sup> fresh weight (fw) and 0.8 mg GAE g<sup>−1</sup> fw for orange and spinach, respectively. MSE substantially increased the phenolic compounds yields (1-fold for orange and 2-fold for spinach) compared with ultrasound-assisted extraction. Furthermore, the antioxidant activity of orange and spinach extracts was evaluated using DPPH, FRAP and ABTS. The obtained results pointed out that the evaluated orange and spinach residues provided extracts with antioxidant activity (2.27 mg TE g<sup>−1</sup> and 0.04 mg TE g<sup>−1</sup>, respectively).María Fernanda Montenegro-LandívarPaulina Tapia-QuirósXanel VecinoMònica ReigCésar ValderramaMercè GranadosJosé Luis CortinaJavier SaurinaMDPI AGarticleagri-food wastesmechanical stirring extractionantioxidant activitywaste to resourcesresource recoveryTherapeutics. PharmacologyRM1-950ENAntioxidants, Vol 10, Iss 1800, p 1800 (2021)
institution DOAJ
collection DOAJ
language EN
topic agri-food wastes
mechanical stirring extraction
antioxidant activity
waste to resources
resource recovery
Therapeutics. Pharmacology
RM1-950
spellingShingle agri-food wastes
mechanical stirring extraction
antioxidant activity
waste to resources
resource recovery
Therapeutics. Pharmacology
RM1-950
María Fernanda Montenegro-Landívar
Paulina Tapia-Quirós
Xanel Vecino
Mònica Reig
César Valderrama
Mercè Granados
José Luis Cortina
Javier Saurina
Recovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity
description Phenolic compounds recovery by mechanical stirring extraction (MSE) was studied from orange and spinach wastes using water as a solvent. The statistical analysis showed that the highest total polyphenol content (TPC) yield was obtained using 15 min, 70 °C, 1:100 (<i>w/v</i>) solid/solvent ratio and pH 4 for orange; and 5 min, 50 °C, 1:50 (<i>w/v</i>) solid/solvent ratio and pH 6 for spinach. Under these conditions, the TPC was 1 mg gallic acid equivalent (GAE) g<sup>−1</sup> fresh weight (fw) and 0.8 mg GAE g<sup>−1</sup> fw for orange and spinach, respectively. MSE substantially increased the phenolic compounds yields (1-fold for orange and 2-fold for spinach) compared with ultrasound-assisted extraction. Furthermore, the antioxidant activity of orange and spinach extracts was evaluated using DPPH, FRAP and ABTS. The obtained results pointed out that the evaluated orange and spinach residues provided extracts with antioxidant activity (2.27 mg TE g<sup>−1</sup> and 0.04 mg TE g<sup>−1</sup>, respectively).
format article
author María Fernanda Montenegro-Landívar
Paulina Tapia-Quirós
Xanel Vecino
Mònica Reig
César Valderrama
Mercè Granados
José Luis Cortina
Javier Saurina
author_facet María Fernanda Montenegro-Landívar
Paulina Tapia-Quirós
Xanel Vecino
Mònica Reig
César Valderrama
Mercè Granados
José Luis Cortina
Javier Saurina
author_sort María Fernanda Montenegro-Landívar
title Recovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity
title_short Recovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity
title_full Recovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity
title_fullStr Recovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity
title_full_unstemmed Recovery of Added-Value Compounds from Orange and Spinach Processing Residues: Green Extraction of Phenolic Compounds and Evaluation of Antioxidant Activity
title_sort recovery of added-value compounds from orange and spinach processing residues: green extraction of phenolic compounds and evaluation of antioxidant activity
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/7d523a7c4f1c4bb2833acf3b25d46ec6
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