Effect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide

The study aimed to investigate the effect of processing temperature and the content of multi-wall carbon nanotubes (MWCNTs) on the rheological, thermal, and electrical properties of polyphenylene sulfide (PPS)/MWCNT nanocomposites. It was observed that the increase in MWCNT content influenced the in...

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Autores principales: Kamil Dydek, Paulina Latko-Durałek, Agata Sulowska, Michał Kubiś, Szymon Demski, Paulina Kozera, Bogna Sztorch, Anna Boczkowska
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Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:d41c7640b01246428e53166121b329262021-11-11T18:48:14ZEffect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide10.3390/polym132138162073-4360https://doaj.org/article/d41c7640b01246428e53166121b329262021-11-01T00:00:00Zhttps://www.mdpi.com/2073-4360/13/21/3816https://doaj.org/toc/2073-4360The study aimed to investigate the effect of processing temperature and the content of multi-wall carbon nanotubes (MWCNTs) on the rheological, thermal, and electrical properties of polyphenylene sulfide (PPS)/MWCNT nanocomposites. It was observed that the increase in MWCNT content influenced the increase of the complex viscosity, storage modulus, and loss modulus. The microscopic observations showed that with an increase in the amount of MWCNTs, the areal ratio of their agglomerates decreases. Thermogravimetric analysis showed no effect of processing temperature and MWCNT content on thermal stability; however, an increase in stability was observed as compared to neat PPS. The differential scanning calorimetry was used to assess the influence of MWCNT addition on the crystallization phenomenon of PPS. The calorimetry showed that with increasing MWCNT content, the degree of crystallinity and crystallization temperature rises. Thermal diffusivity tests proved that with an increase in the processing temperature and the content of MWCNTs, the diffusivity also increases and declines at higher testing temperatures. The resistivity measurements showed that the conductivity of the PPS/MWCNT nanocomposite increases with the increase in MWCNT content. The processing temperature did not affect resistivity.Kamil DydekPaulina Latko-DurałekAgata SulowskaMichał KubiśSzymon DemskiPaulina KozeraBogna SztorchAnna BoczkowskaMDPI AGarticlePPScarbon nanotubesthermal analysiselectrical propertiesrheological propertiesOrganic chemistryQD241-441ENPolymers, Vol 13, Iss 3816, p 3816 (2021)
institution DOAJ
collection DOAJ
language EN
topic PPS
carbon nanotubes
thermal analysis
electrical properties
rheological properties
Organic chemistry
QD241-441
spellingShingle PPS
carbon nanotubes
thermal analysis
electrical properties
rheological properties
Organic chemistry
QD241-441
Kamil Dydek
Paulina Latko-Durałek
Agata Sulowska
Michał Kubiś
Szymon Demski
Paulina Kozera
Bogna Sztorch
Anna Boczkowska
Effect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide
description The study aimed to investigate the effect of processing temperature and the content of multi-wall carbon nanotubes (MWCNTs) on the rheological, thermal, and electrical properties of polyphenylene sulfide (PPS)/MWCNT nanocomposites. It was observed that the increase in MWCNT content influenced the increase of the complex viscosity, storage modulus, and loss modulus. The microscopic observations showed that with an increase in the amount of MWCNTs, the areal ratio of their agglomerates decreases. Thermogravimetric analysis showed no effect of processing temperature and MWCNT content on thermal stability; however, an increase in stability was observed as compared to neat PPS. The differential scanning calorimetry was used to assess the influence of MWCNT addition on the crystallization phenomenon of PPS. The calorimetry showed that with increasing MWCNT content, the degree of crystallinity and crystallization temperature rises. Thermal diffusivity tests proved that with an increase in the processing temperature and the content of MWCNTs, the diffusivity also increases and declines at higher testing temperatures. The resistivity measurements showed that the conductivity of the PPS/MWCNT nanocomposite increases with the increase in MWCNT content. The processing temperature did not affect resistivity.
format article
author Kamil Dydek
Paulina Latko-Durałek
Agata Sulowska
Michał Kubiś
Szymon Demski
Paulina Kozera
Bogna Sztorch
Anna Boczkowska
author_facet Kamil Dydek
Paulina Latko-Durałek
Agata Sulowska
Michał Kubiś
Szymon Demski
Paulina Kozera
Bogna Sztorch
Anna Boczkowska
author_sort Kamil Dydek
title Effect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide
title_short Effect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide
title_full Effect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide
title_fullStr Effect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide
title_full_unstemmed Effect of Processing Temperature and the Content of Carbon Nanotubes on the Properties of Nanocomposites Based on Polyphenylene Sulfide
title_sort effect of processing temperature and the content of carbon nanotubes on the properties of nanocomposites based on polyphenylene sulfide
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/d41c7640b01246428e53166121b32926
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