Valorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction

The table olive industry is producing a huge amount of wastewater, which is a post-processing cost and an environmental concern. The present study aims to valorize this processing by-product to obtain a value-added product, thereby enhancing resource efficiency and contributing to achieving sustaina...

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Autores principales: Alberto J. Huertas-Alonso, Mohsen Gavahian, Diego J. González-Serrano, Milad Hadidi, Manuel Salgado-Ramos, M. Prado Sánchez-Verdú, Mario J. Simirgiotis, Francisco J. Barba, Daniel Franco, José M. Lorenzo, Andrés Moreno
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Lenguaje:EN
Publicado: MDPI AG 2021
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NMR
HMF
Acceso en línea:https://doaj.org/article/fde2d280d2904ca0bf6641d8197686d4
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spelling oai:doaj.org-article:fde2d280d2904ca0bf6641d8197686d42021-11-25T16:25:22ZValorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction10.3390/antiox101116522076-3921https://doaj.org/article/fde2d280d2904ca0bf6641d8197686d42021-10-01T00:00:00Zhttps://www.mdpi.com/2076-3921/10/11/1652https://doaj.org/toc/2076-3921The table olive industry is producing a huge amount of wastewater, which is a post-processing cost and an environmental concern. The present study aims to valorize this processing by-product to obtain a value-added product, thereby enhancing resource efficiency and contributing to achieving sustainable development goals (SDGs). In this sense, a chemical reaction-based platform was developed to obtain valuable components, such as levulinic acid (LA) and 5-hydromethylfurfural (HMF). The products were then analyzed using NMR identification of the antioxidant phenolic fraction and microwave single-phase reaction of the sugary fraction. According to the results, the highest concentration of phenolic compounds does not correspond to the sample directly obtained from NaOH treatment (S1), indicating that water washing steps (S2–S5) are fundamental to recover phenolic substances. Moreover, glucose was presented in the sugary fraction that can be transformed into levulinic acid by a single-phase reaction under microwave irradiation. The information provided in this manuscript suggests that the wastewater from the olive processing industry can be valorized to obtain valuable products.Alberto J. Huertas-AlonsoMohsen GavahianDiego J. González-SerranoMilad HadidiManuel Salgado-RamosM. Prado Sánchez-VerdúMario J. SimirgiotisFrancisco J. BarbaDaniel FrancoJosé M. LorenzoAndrés MorenoMDPI AGarticlewaste valorizationtable olive wastewaterNMRphenolic compoundslevulinic acidHMFTherapeutics. PharmacologyRM1-950ENAntioxidants, Vol 10, Iss 1652, p 1652 (2021)
institution DOAJ
collection DOAJ
language EN
topic waste valorization
table olive wastewater
NMR
phenolic compounds
levulinic acid
HMF
Therapeutics. Pharmacology
RM1-950
spellingShingle waste valorization
table olive wastewater
NMR
phenolic compounds
levulinic acid
HMF
Therapeutics. Pharmacology
RM1-950
Alberto J. Huertas-Alonso
Mohsen Gavahian
Diego J. González-Serrano
Milad Hadidi
Manuel Salgado-Ramos
M. Prado Sánchez-Verdú
Mario J. Simirgiotis
Francisco J. Barba
Daniel Franco
José M. Lorenzo
Andrés Moreno
Valorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction
description The table olive industry is producing a huge amount of wastewater, which is a post-processing cost and an environmental concern. The present study aims to valorize this processing by-product to obtain a value-added product, thereby enhancing resource efficiency and contributing to achieving sustainable development goals (SDGs). In this sense, a chemical reaction-based platform was developed to obtain valuable components, such as levulinic acid (LA) and 5-hydromethylfurfural (HMF). The products were then analyzed using NMR identification of the antioxidant phenolic fraction and microwave single-phase reaction of the sugary fraction. According to the results, the highest concentration of phenolic compounds does not correspond to the sample directly obtained from NaOH treatment (S1), indicating that water washing steps (S2–S5) are fundamental to recover phenolic substances. Moreover, glucose was presented in the sugary fraction that can be transformed into levulinic acid by a single-phase reaction under microwave irradiation. The information provided in this manuscript suggests that the wastewater from the olive processing industry can be valorized to obtain valuable products.
format article
author Alberto J. Huertas-Alonso
Mohsen Gavahian
Diego J. González-Serrano
Milad Hadidi
Manuel Salgado-Ramos
M. Prado Sánchez-Verdú
Mario J. Simirgiotis
Francisco J. Barba
Daniel Franco
José M. Lorenzo
Andrés Moreno
author_facet Alberto J. Huertas-Alonso
Mohsen Gavahian
Diego J. González-Serrano
Milad Hadidi
Manuel Salgado-Ramos
M. Prado Sánchez-Verdú
Mario J. Simirgiotis
Francisco J. Barba
Daniel Franco
José M. Lorenzo
Andrés Moreno
author_sort Alberto J. Huertas-Alonso
title Valorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction
title_short Valorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction
title_full Valorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction
title_fullStr Valorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction
title_full_unstemmed Valorization of Wastewater from Table Olives: NMR Identification of Antioxidant Phenolic Fraction and Microwave Single-Phase Reaction of Sugary Fraction
title_sort valorization of wastewater from table olives: nmr identification of antioxidant phenolic fraction and microwave single-phase reaction of sugary fraction
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/fde2d280d2904ca0bf6641d8197686d4
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