INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY

We report on the influence of temperature, mixing ratio and holding time of NaOH & KOH intercalations on the surface area, micropore volume and micropore width of pre-baked clay samples. Pore size & surface area analyzer was used to measure the surface area, micropore volume and aver...

Descripción completa

Guardado en:

Detalles Bibliográficos
Autores principales:	AHMAD,IMTIAZ, ULLAH,HAMEED
Lenguaje:	English
Publicado:	Sociedad Chilena de Química 2009
Materias:	clay baked clay activation intercalation dubinin-radushkevich (DR) method
Acceso en línea:	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072009000300005
Etiquetas:	Agregar Etiqueta Sin Etiquetas, Sea el primero en etiquetar este registro!

id	oai:scielo:S0717-97072009000300005
record_format	dspace
spelling	oai:scielo:S0717-970720090003000052010-03-17INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAYAHMAD,IMTIAZULLAH,HAMEED clay baked clay activation intercalation dubinin-radushkevich (DR) method We report on the influence of temperature, mixing ratio and holding time of NaOH & KOH intercalations on the surface area, micropore volume and micropore width of pre-baked clay samples. Pore size & surface area analyzer was used to measure the surface area, micropore volume and average pore width using Dubinin-Radushkevich (DR) method. A meaning full effect was observed when the temperature was increased from ambient up to 150 °C in case of both intercalating agents. Increasing temperature beyond 150 °C caused a decline in surface area generation even up to 750 °C. The results also show that mixing ratio has a positive effect on the porosity and the micropore surface area inereases as the mixing ratio inereases in case of both intercalating agents. The influence of holding time shows two different trends. In case of NaOH, the porosity inereases as the time inereases while in case of KOH, the porosity decreases as the time inereases. SEM, EDX and XRD studies were also performed. The results show effective insertion of the sodium and potassium into the clay matrix thereby causing generation of porosity.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.54 n.3 20092009-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072009000300005en10.4067/S0717-97072009000300005
institution	Scielo Chile
collection	Scielo Chile
language	English
topic	clay baked clay activation intercalation dubinin-radushkevich (DR) method
spellingShingle	clay baked clay activation intercalation dubinin-radushkevich (DR) method AHMAD,IMTIAZ ULLAH,HAMEED INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY
description	We report on the influence of temperature, mixing ratio and holding time of NaOH & KOH intercalations on the surface area, micropore volume and micropore width of pre-baked clay samples. Pore size & surface area analyzer was used to measure the surface area, micropore volume and average pore width using Dubinin-Radushkevich (DR) method. A meaning full effect was observed when the temperature was increased from ambient up to 150 °C in case of both intercalating agents. Increasing temperature beyond 150 °C caused a decline in surface area generation even up to 750 °C. The results also show that mixing ratio has a positive effect on the porosity and the micropore surface area inereases as the mixing ratio inereases in case of both intercalating agents. The influence of holding time shows two different trends. In case of NaOH, the porosity inereases as the time inereases while in case of KOH, the porosity decreases as the time inereases. SEM, EDX and XRD studies were also performed. The results show effective insertion of the sodium and potassium into the clay matrix thereby causing generation of porosity.
author	AHMAD,IMTIAZ ULLAH,HAMEED
author_facet	AHMAD,IMTIAZ ULLAH,HAMEED
author_sort	AHMAD,IMTIAZ
title	INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY
title_short	INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY
title_full	INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY
title_fullStr	INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY
title_full_unstemmed	INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY
title_sort	influence of some intercalations on activation of pre-baked clay
publisher	Sociedad Chilena de Química
publishDate	2009
url	http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072009000300005
work_keys_str_mv	AT ahmadimtiaz influenceofsomeintercalationsonactivationofprebakedclay AT ullahhameed influenceofsomeintercalationsonactivationofprebakedclay
_version_	1718445406718787584

INFLUENCE OF SOME INTERCALATIONS ON ACTIVATION OF PRE-BAKED CLAY

Ejemplares similares